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Record W2508649431 · doi:10.1021/acs.chemmater.5b01844

Biotemplated Silica and Silicon Materials as Building Blocks for Micro- to Nanostructures

2015· article· en· W2508649431 on OpenAlexfundno aff
Noémie‐Manuelle Dorval Courchesne, Stephen A. Steiner, Victor Cantu, Paula T. Hammond, Angela M. Belcher

Bibliographic record

VenueChemistry of Materials · 2015
Typearticle
Languageen
FieldMaterials Science
TopicDiatoms and Algae Research
Canadian institutionsnot available
FundersNatural Sciences and Engineering Research Council of CanadaDefense Advanced Research Projects AgencyEniMassachusetts Institute of Technology
KeywordsMaterials scienceNanotechnologySiliconNanostructureNanoporousEtching (microfabrication)WaferNanoporeNanowireIsotropic etchingAnodizingLithographyAluminiumOptoelectronicsLayer (electronics)Metallurgy

Abstract

fetched live from OpenAlex

Silicon is essential in several energy-related devices, including solar cells, batteries, and some electrochemical systems. These devices often rely on micro- or nanostructures to function efficiently, and require patterning of metallic surfaces. Currently, constructing silicon features at the micro- and nanoscale requires top-down energy-intensive processes, such as e-beam lithography, chemical etching, or anodization. While it is difficult to form silicon in aqueous solution, its oxide, silica, can easily be synthesized using sol–gel chemistry and nucleated onto templates with diverse shapes to create porous or continuous architectures. Here, we demonstrate that novel silica nanostructures can be synthesized via biomineralization, and that they can be reduced to silicon using magnesiothermal reduction. We selected three biotemplates to create silica structures with various aspect ratios and length scales. First, we use diatomaceous earth as a model silica material to optimize our process, and we also biomineralize silica onto two microorganisms, the high aspect ratio M13 bacteriophage, and the helical Spirulina major algae. During our process, the shape of the materials is preserved, resulting in silicon nanowires, nanoporous networks, spirals, and other micro- and nanostructures with high surface area. Our method provides an alternative for the creation of silicon nanostructures, using preformed silica synthesized in solution. The process could be extended to a broader range of microorganisms and metal oxides for the rational design of on-demand micro- and nanostructured metals. In addition, we show that the intrinsic composition of the biotemplates as well as their growth medium can introduce impurities that could potentially be used as dopants in the final silicon structures, and that could allow for tuning the composition of n-doped or p-doped biotemplated silicon for use as semiconducting building blocks.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.023
GPT teacher head0.303
Teacher spread0.280 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations22
Published2015
Admission routes1
Has abstractyes

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