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Record W2531581264 · doi:10.1021/acssuschemeng.6b01674

Diffusion-Controlled Simultaneous Sensing and Scavenging of Heavy Metal Ions in Water Using Atomically Precise Cluster–Cellulose Nanocrystal Composites

2016· article· en· W2531581264 on OpenAlexafffund
Nishil Mohammed, Avijit Baidya, Vasanthanarayan Murugesan, Avula Anil Kumar, Mohd Azhardin Ganayee, Jyoti Sarita Mohanty, Kam Chiu Tam, Thalappil Pradeep

Bibliographic record

VenueACS Sustainable Chemistry & Engineering · 2016
Typearticle
Languageen
FieldMaterials Science
TopicNanocluster Synthesis and Applications
Canadian institutionsUniversity of Waterloo
FundersNatural Sciences and Engineering Research Council of CanadaMitacsCanada Foundation for Innovation
KeywordsNanoclustersMetal ions in aqueous solutionNanocrystalMaterials scienceX-ray photoelectron spectroscopyNanocompositeChemical engineeringCelluloseAdsorptionIonMetalNanotechnologyAnalytical Chemistry (journal)ChemistryPhysical chemistryMetallurgyOrganic chemistry

Abstract

fetched live from OpenAlex

Development of a system that can simultaneously sense and scavenge toxic heavy metal ions at low concentrations is an ideal solution for in situ monitoring and purification of contaminated water. In this paper, we report on the synthesis and application of a novel system, luminescent atomically precise cluster–cellulose nanocrystal composite, namely, bovine serum albumin-protected gold nanoclusters (Au@BSA NCs)-loaded cellulose nanocrystal–alginate hydrogel beads, that can simultaneously sense and scavenge heavy metal ions, specifically mercury ions in water. Characterization of the system performed using scanning electron microscopy coupled with energy dispersive spectroscopy and X-ray photoelectron spectroscopy elucidated the physical and chemical characteristics of the system. Additionally, we proposed a new method to visualize the diffusion phenomenon and calculate the effective diffusion coefficient of heavy metal ions in hydrogel beads by monitoring the fluorescence-quenching dynamics of Au@BSA NCs upon binding with mercury ions. Finally, practical applications of this nanocomposite were demonstrated using batch adsorption experiments as well as using a dip pen device loaded with the hydrogel beads for in situ monitoring of heavy metal ions in water.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.004
GPT teacher head0.190
Teacher spread0.186 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations78
Published2016
Admission routes2
Has abstractyes

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Same venueACS Sustainable Chemistry & EngineeringSame topicNanocluster Synthesis and ApplicationsFrench-language works237,207