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Record W2532932341 · doi:10.1180/minmag.2016.080.042

Lead-tellurium oxysalts from Otto Mountain near Baker, California, USA: XII. Andychristyite, PbCu<sup>2+</sup>Te<sup>6+</sup>O<sub>5</sub>(H<sub>2</sub>O), a new mineral with<i>hcp</i>stair-step layers

2016· article· en· W2532932341 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueMineralogical Magazine · 2016
Typearticle
Languageen
FieldMaterials Science
TopicCrystal Structures and Properties
Canadian institutionsUniversity of Manitoba
FundersUniversity of ManitobaCalifornia Institute of TechnologyIan Potter FoundationNational Science Foundation
KeywordsTellurateTriclinic crystal systemPleochroismMohs scale of mineral hardnessCrystallographyQuartzElectron microprobeMineralOctahedronChemistryMonoclinic crystal systemRaman spectroscopyOrthorhombic crystal systemMineralogyCrystal structureMaterials scienceMetallurgy

Abstract

fetched live from OpenAlex

Abstract Andychristyite, PbCu 2+ Te 6+ O5(H 2 O), is a new tellurate mineral from Otto Mountain near Baker, California, USA. It occurs in vugs in quartz in association with timroseite. It is interpreted as having formed from the partial oxidation of primary sulfides and tellurides during or following brecciation of quartz veins. Andychristyite is triclinic, space group P1̄, with unit-cell dimensions a = 5.322(3), b = 7.098(4), c = 7.511 (4) Å, α = 83.486(7), β = 76.279(5), γ = 70.742(5)°, V = 260.0(2) Å3 and Z = 2. It forms as small tabular crystals up to ∼50 μm across, in sub-parallel aggregates. The colour is bluish green and the streak is very pale bluish green. Crystals are transparent with adamantine lustre. The Mohs hardness is estimated at between 2 and 3. Andychristyite is brittle with an irregular fracture and one perfect cleavage on {001}. The calculated density based on the empirical formula is 6.304 g/cm 3 . The mineral is optically biaxial, with large 2V, strong dispersion, and moderate very pale blue-green to medium blue-green pleochroism. The electron microprobe analyses (average of five) provided: PbO 43.21, CuO 15.38, TeO 3 35.29, H 2 O 3.49 (structure), total 97.37 wt.%. The empirical formula (based on 6 O apfu) is: Pb 0.98 Cu 2+ 0.98 Te 6+ 1.02 O 6 H 1.96 . The Raman spectrum exhibits prominent features consistent with the mineral being a tellurate, as well as an OH stretching feature confirming a hydrous component. The eight strongest powder X-ray diffraction lines are [ d obs in Å( I )( hkl )]: 6.71(16)(010), 4.76(17)(110), 3.274(100)(120,102,012), 2.641(27)(102, 211, 112), 2.434(23)(multiple), 1.6736(17)(multiple), 1.5882(21)(multiple) and 1.5133(15)(multiple). The crystal structure of andychristyite (R 1 = 0.0165 for 1511 reflections with F o &gt; 4σ F ) consists of stair-step-like hcp polyhedral layers of Te 6+ O 6 and Cu 2+ O 6 octahedra parallel to {001}, which are linked in the [001] direction by bonds to interlayer Pb atoms. The structures of eckhardite, bairdite, timroseite and paratimroseite also contain stair-step-like hcp polyhedral layers.

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Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.462
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0020.001
Meta-epidemiology (broad)0.0020.001
Bibliometrics0.0000.001
Science and technology studies0.0010.001
Scholarly communication0.0010.001
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0020.004

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.209
Teacher spread0.195 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it