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Record W2534400021 · doi:10.1021/acs.iecr.6b03122

Modeling and Optimization of Protein PEGylation

2016· article· en· W2534400021 on OpenAlexafffund
Xiaojiao Shang, Brandon Corbett, Brian Macdonald, Prashant Mhaskar, Raja Ghosh

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2016
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicProtein purification and stability
Canadian institutionsMcMaster University
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsPEGylationPolyethylene glycolPEG ratioProcess (computing)ChemistryComputer scienceProcess optimizationBiological systemChemical engineeringOrganic chemistryEngineeringBiology

Abstract

fetched live from OpenAlex

A PEGylated protein is prepared by conjugating polyethylene glycol (or PEG) with the protein, a process known as PEGylation. Most PEGylation processes lead to synthesis of different PEGylated forms of the protein, among which only one form is typically of interest. In this work, we propose a modeling and optimization-based approach for determining optimal operating conditions for protein PEGylation. To this end, a first-principles model is proposed and targeted experiments are carried out to estimate the model parameters. A simulation-based optimization is then carried out to suggest the best operating conditions. Specifically, results suggest that to maximize the concentration of mono-PEGylated product, the reaction should be carried out at high pH and with a high ratio of PEG to protein. Subsequent experiments are conducted to confirm the validity of the modeling and optimization approach.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Simulation or modeling · Consensus signal: Simulation or modeling
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.006
Threshold uncertainty score0.012

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0010.001
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.067
GPT teacher head0.312
Teacher spread0.245 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designSimulation or modeling
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations11
Published2016
Admission routes2
Has abstractyes

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