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Structures, Phase Transitions and Tricritical Behavior of the Hybrid Perovskite Methyl Ammonium Lead Iodide

2016· article· en· 567 citations· W2537132801 on OpenAlex· 10.1038/srep35685

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A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

Canadian funderA Canadian agency funded it. The work may carry no Canadian affiliation at all.

No Canadian affiliation. An affiliation-only frame — the usual design — would never have seen this work. It is one of the works that make the case for inverting the frame.

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Opus teacher head0.012
GPT teacher head0.250
Teacher spread
0.238 · how far apart the two teachers sit on this one work
Validation status
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Abstract

Abstract We have examined the crystal structures and structural phase transitions of the deuterated, partially deuterated and hydrogenous organic-inorganic hybrid perovskite methyl ammonium lead iodide (MAPbI 3 ) using time-of-flight neutron and synchrotron X-ray powder diffraction. Near 330 K the high temperature cubic phases transformed to a body-centered tetragonal phase. The variation of the order parameter Q for this transition scaled with temperature T as Q ∼ (T c −T) β , where T c is the critical temperature and the exponent β was close to ¼, as predicted for a tricritical phase transition. However, we also observed coexistence of the cubic and tetragonal phases over a range of temperature in all cases, demonstrating that the phase transition was in fact first-order, although still very close to tricritical. Upon cooling further, all the tetragonal phases transformed into a low temperature orthorhombic phase around 160 K, again via a first-order phase transition. Based upon these results, we discuss the impact of the structural phase transitions upon photovoltaic performance of MAPbI 3 based solar cells.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

The record

Venue
Scientific Reports
Topic
Perovskite Materials and Applications
Field
Engineering
Canadian institutions
Funders
Office of ScienceArgonne National LaboratoryBasic Energy SciencesUT-BattelleOak Ridge National LaboratoryBrigham Young UniversityBattelleUniversity of TorontoLaboratory Directed Research and DevelopmentU.S. Department of Energy
Keywords
Tetragonal crystal systemPhase transitionPerovskite (structure)Orthorhombic crystal systemMaterials scienceIodidePhase (matter)Ammonium iodideNeutron diffractionCrystallographyDeuteriumCritical exponentCrystal structureChemistryCondensed matter physicsInorganic chemistryPhysicsOrganic chemistry
Has abstract in OpenAlex
yes