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Record W2555144365 · doi:10.4052/tigg.14.13

Glycosynthases: New Tools for Oligosaccharide Synthesis.

2002· article· en· W2555144365 on OpenAlexafffund
David L. Jakeman, Stephen G. Withers

Bibliographic record

VenueTrends in Glycoscience and Glycotechnology · 2002
Typearticle
Languageen
FieldChemistry
TopicCarbohydrate Chemistry and Synthesis
Canadian institutionsUniversity of British Columbia
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsOligosaccharideChemistryComputational biologyBiochemistryComputer scienceBiology

Abstract

fetched live from OpenAlex

生命現象におけるオリゴ糖鎖の多様な働きが次々と明らかにされている。オリゴ糖の持つ生理活性をより深く理解し利用していくためには、天然型および非天然型オリゴ糖を入手する必要がある。したがって、オリゴ糖合成は化学における最も活発に研究されている分野の一つとなっている。ここで紹介するグリコシンターゼは全く新しいタイプの変異酵素であり、有機化学的な方法や糖転移酵素を用いる従来法と共に、オリゴ糖合成に利用することができる。グリコシンターゼとは、糖加水分解酵素の触媒部位の求核性アミノ酸を非求核性アミノ酸で置換した変異体のことであり、加水分解に対して不活性である。しかし、糖受容体の存在下、糖-酵素中間体に類似した構造をもつ糖供与体に作用させると、高収率で糖転移反応を進行させることができる。本総説は、筆者の研究室で開発された一連のグリコシンターゼを用いた最近の結果をまとめたものである (JACS, 1998, 120, 5583-5584)。いくつかの糖供与体をさまざまな糖受容体に転移させることを目的として、数種類の加水分解酵素に対して変異導入を行った。また、あるグリコシンターゼに関しては、糖転移反応速度の向上が図られた。このことによって、グリコシンターゼを利用する広範なオリゴ糖合成が可能となった。

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.717
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0030.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.056
GPT teacher head0.265
Teacher spread0.209 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations44
Published2002
Admission routes2
Has abstractyes

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