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Record W2557330709 · doi:10.1002/ejic.201600468

Design and Photophysical Studies of Acridine‐Based Ru<sup>II</sup> Complexes for Applications as DNA Photoprobes

2016· article· en· W2557330709 on OpenAlexaff
Quentin Deraedt, Lionel Marcélis, Thomas Auvray, Garry S. Hanan, Frédérique Loiseau, Benjamin Elias

Bibliographic record

VenueEuropean Journal of Inorganic Chemistry · 2016
Typearticle
Languageen
FieldMedicine
TopicMetal complexes synthesis and properties
Canadian institutionsUniversité de MontréalCegep Edouard Montpetit
FundersUniversité Catholique de LouvainFonds De La Recherche Scientifique - FNRSBelgian American Educational Foundation
KeywordsAcridinePhenazineChemistryExcited stateHydrogen bondMoleculePhotochemistryLuminescenceDNAStereochemistryCrystallographyOrganic chemistry

Abstract

fetched live from OpenAlex

A series of new extended planar aromatic ligands based on an acridine core (dpac = dipyrido[3,2‐ a :2′,3′‐ c ]acridine; dpacF 2 = 7,8‐difluorodipyrido[3,2‐ a :2′,3′‐ c ]acridine; dpacF 4 = 6,7,8,9‐tetrafluorodipyrido[3,2‐ a :2′,3′‐ c ]acridine) and their respective Ru II complexes were synthesized and extensively studied. The photophysical and theoretical studies revealed that Ru‐DPAC and Ru‐DPACF 2 allow emission from a 3 MLCT phen/dpac excited state at 597 and 604 nm, respectively, whereas the lowest excited state for Ru‐DPACF 4 shifts from a bright 3 MLCT phen/dpac state towards a poorly luminescent 3 MLCT dpac state ( λ em = 609 nm) owing to the formation of hydrogen bonds with water molecules in the excited state. These complexes exhibit up to sevenfold luminescence enhancement in the presence of complementary and mismatched DNA, demonstrating a strong binding to polynucleotides. The results emphasize the interest in Ru II complexes bearing acridine derivatives as DNA interacting agents as a complement to the well‐known phenazine‐based derivatives.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.005
Threshold uncertainty score0.434

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.062
GPT teacher head0.286
Teacher spread0.224 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations12
Published2016
Admission routes1
Has abstractyes

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Same venueEuropean Journal of Inorganic ChemistrySame topicMetal complexes synthesis and propertiesFrench-language works237,207