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Record W2571744180 · doi:10.1021/acs.jpcc.6b11675

Effects of Side-Chain Length and Shape on Polytellurophene Molecular Order and Blend Morphology

2017· article· en· W2571744180 on OpenAlexaff
Joseph Razzell Hollis, Franziska D. Fleischli, Ashlee A. Jahnke, Natalie Stingelin, Dwight S. Seferos, Ji‐Seon Kim

Bibliographic record

VenueThe Journal of Physical Chemistry C · 2017
Typearticle
Languageen
FieldEngineering
TopicOrganic Electronics and Photovoltaics
Canadian institutionsUniversity of Toronto
FundersEngineering and Physical Sciences Research Council
KeywordsRaman spectroscopySide chainMaterials sciencePolythiophenePolymerConjugated systemAlkylOrganic electronicsSteric effectsChemical physicsPhase (matter)CrystallographyTransistorChemistryConductive polymerStereochemistryOrganic chemistryOpticsComposite material

Abstract

fetched live from OpenAlex

High Resolution Image Download MS PowerPoint Slide We investigate the molecular order and thin film morphology of the conjugated polymer polytellurophene, in order to understand how the tellurium atom and the choice of side-chain influence the conjugated polymer’s backbone planarity and performance in organic transistors. We find that poly(3hexyltellurophene) (P3HTe) continues the trend from polythiophene (P3HT) to polyselenophene (P3HS): substitution with Tellurium leads to a more planar backbone, evident from the shifts of the C═C vibrational peak to lower wavenumbers (∼1389 cm –1 ) and a smaller optical band gap (∼1.4 eV). Resonant Raman spectroscopy revealed that molecular order was highly dependent on the structure of the P3ATe alkyl side-chain: a longer chains introduces kinetic hindrance, reducing the fraction of ordered phase obtained at room temperature, while a branched side-chain introduces steric hindrance, with intrinsic disorder present even when deposited at higher temperatures. When blended with the insulator HDPE, all three polymers exhibit little additional disorder and instead form phase-separated networks of high molecular order that are beneficial to percolated charge transport in transistors. We find that molecular order, as measured by Raman, correlates well with reported transistor mobilities and provides a greater understanding of the structure–property relationships that determine the performance of these novel organometallic polymers in electronic devices.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score0.276

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.003
GPT teacher head0.198
Teacher spread0.195 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations36
Published2017
Admission routes1
Has abstractyes

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