Bibliographic record
Abstract
This is an unusually brief editorial -and I apologize for that -but annual leave, backlog and family commitments are hoovering up most of my time, so I will go straight to the heart of our new SYNFORM issue, whose quality has definitely not been affected by the holiday period.The first article is from the group of L. Gooßen (Germany) with his new highly effective method for incorporating the SCF 3 function into organic molecules.The second contribution comes from S. Canesi (Canada) whose group has developed a new approach to the synthesis of the alkaloid strychnine mediated by hypervalent iodine reagents.The third article is a Young Career Focus with M. von Delius (Germany) who answers the usual set of questions about his views on organic chemistry, his career so far and professional ambitions.The issue is closed by the new photoredox approach to nitrones from nitro compounds developed by B.-C. Hong (Taiwan).Enjoy your reading!In this issue SYNLETT Highlight Metal-Free Trifluoromethylthiolation of Alkyl Electrophiles via a Cascade of Thiocyanation and Nucleophilic CyanideCF 3 Substitution . . . . . . . . . . . . . . . . . .
Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.
How this classification was reachedexpand
Full frame machine prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.
Distilled classifier scores by category (both heads)
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.002 | 0.008 |
| Meta-epidemiology (narrow) | 0.001 | 0.000 |
| Meta-epidemiology (broad) | 0.001 | 0.001 |
| Bibliometrics | 0.002 | 0.001 |
| Science and technology studies | 0.001 | 0.001 |
| Scholarly communication | 0.007 | 0.003 |
| Open science | 0.002 | 0.002 |
| Research integrity | 0.004 | 0.003 |
| Insufficient payload (model declined to judge) | 0.417 | 0.284 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; the direct Gemma label and the distilled Codex classifier agree on what is shown here.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".