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Record W2611270003 · doi:10.1002/lom3.10186

Methodological biases in estimates of macroalgal macromolecular composition

2017· article· en· W2611270003 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueLimnology and Oceanography Methods · 2017
Typearticle
Languageen
FieldAgricultural and Biological Sciences
TopicSeaweed-derived Bioactive Compounds
Canadian institutionsMount Allison University
FundersCanada Research ChairsNew Brunswick Innovation FoundationGordon and Betty Moore Foundation
KeywordsMacromoleculeCarbohydrateExtraction (chemistry)ChemistryNitrogenSample preparationComposition (language)Food scienceChromatographyBiochemistry

Abstract

fetched live from OpenAlex

Abstract Interest surrounding the use of macroalgae macromolecules for food products, biofuels, or other industrial applications is growing. As researchers search for macroalgae with especially high protein, lipid, carbohydrate or fibre content, the demand for a suite of standardized and unbiased methods for quantifying macroalgae macromolecules increases. Using data from available scientific literature, we evaluated the biases of the major methods used to determine macroalgal macromolecular content, as well as the sample drying methods employed. We found that drying at room temperature prior to analysis resulted in the highest estimates of protein and carbohydrate, and that freeze‐drying provided the highest estimates of lipid. Using nitrogen content and the standard conversion factor to calculate protein in macroalgae (N × 6.25 method) overestimates protein content compared to protein assays such as the Bradford ( ) or Lowry ( ) assays. The Bligh and Dyer ( ) lipid extraction method was found to have a yield nearly two‐fold higher than other standard methods. For carbohydrates, the By Difference and Prosky et al. ( ) methods provide estimates up to five‐fold higher than other common methods used to determine carbohydrate and fibre. Based on these results we recommend using protein assays as opposed to nitrogen content assays to determine protein content, the Bligh and Dyer lipid extraction method for lipids, and the By Difference and Prosky method for carbohydrate and fibre, respectively.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Observational · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.530
Threshold uncertainty score0.317

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.178
GPT teacher head0.405
Teacher spread0.227 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it