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Record W2613131859

High pressure vapour-liquid equilibrium measurement for perfluorinated chemicals using a static analytical apparatus.

2016· dissertation· en· W2613131859 on OpenAlexaboutno aff
Emmanuel. Gande

Bibliographic record

VenueResearchSpace (University of KwaZulu-Natal) · 2016
Typedissertation
Languageen
FieldChemistry
TopicChemical Thermodynamics and Molecular Structure
Canadian institutionsnot available
Fundersnot available
KeywordsVapor–liquid equilibriumThermodynamicsProcess engineeringVapor pressureLiquid liquidAnalytical Chemistry (journal)Materials scienceChemistryPetroleum engineeringChromatographyOrganic chemistryEngineeringPhysics
DOInot available

Abstract

fetched live from OpenAlex

The current study contributes to the continuing research on the measurement and correlation of phase equilibrium data of binary mixtures of 1, 1, 2, 3, 3, 3-hexafluoro-1-propene (R-1216) and alkanes.Fluorinated refrigerants such as R-1216 (not in pure form) are excellent contenders within the next generation of refrigerants that can meet the requirements of Montreal and Kyoto protocols.Since these refrigerants could prove their suitability to be excellent candidates as probable replacements of refrigerants with higher global warming potentials, as such the refrigeration industry is in need of experimental data regarding R-1216 and its mixtures so as to enhance process efficiencies.R-1216 was chosen as the focus of the study because has gained eminence in research activities as it finds use as an intermediate in chemical reactions and as a monomer in the production of polymers among other applications.Within the larger research project, investigations have been undertaken into the experimental measurement of vapour pressures and densities for pure hexafluoropropylene and the measurement of isothermal binary vapour-liquid equilibrium (VLE) data for systems involving R-1216 and alkenes (ethylene, propylene, and 1-butene).And, phase equilibrium data for mixtures involving R1216 with ethane (R-170), propane and n-butane have been measured.This work is a continuation of the work on binary mixtures of R-1216 with alkanes.This study concerned the measurement of isothermal high-pressure binary HPVLE data for mixtures of R-1216 + [n-pentane, n-hexane and n-heptane] at temperatures ranging between 352 -423 K, and pressures up to 3.0 MPa.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.051
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.030
GPT teacher head0.280
Teacher spread0.249 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2016
Admission routes1
Has abstractyes

Explore more

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