Facile Synthesis of α-MnO2 with a 3D Staghorn Coral-like Micro-Structure Assembled by Nano-Rods and Its Application in Electrochemical Supercapacitors
Bibliographic record
Abstract
Abstract: Manganese oxides with an alpha crystal structure are synthesized via combined solid-state reaction and wet chemical processing, which is a simple and inexpensive synthetic route easy for mass production. The effects of the synthetic reaction duration and the temperature of acid treatments on crystal structure, morphology, and electrochemical capacitive properties of α-MnO2 are discussed. It is evidenced that the samples treated in acid for a longer time at 25 °C display the uniform nanorods that are aggregated to form micro-buildings with fine features on the surface of rods. This microstructure possesses large surface areas and more active sites that are easy to access electrochemically, leading to a better electrochemical capacitive performance. We expected that these results would provide the practical information for shape- and morphology-controlled synthesis for nanostructured functional materials in supercapacitor applications.
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How this classification was reachedexpand
Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.000 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.000 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.000 | 0.001 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.001 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.000 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from itClassification
machine, unvalidatedMachine predicted; a candidate call from one teacher head, not a consensus.
How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".