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Record W2621563188

Assessment of Metaborate Fusion for the Rapid Dissolution of Solid Samples: Suitability with the Northstar ARSIIe

2016· article· en· W2621563188 on OpenAlexaboutno aff
Annie Michaud, Dominic Larivière

Bibliographic record

Venuenot available
Typearticle
Languageen
FieldEnvironmental Science
TopicRadioactive contamination and transfer
Canadian institutionsnot available
Fundersnot available
KeywordsDissolutionThoriumPlutoniumUraniumEnvironmental scienceProcess engineeringRadiochemistryChemistryMaterials scienceEngineeringMetallurgy
DOInot available

Abstract

fetched live from OpenAlex

Abstract : The original goal of this project was to develop a rapid dissolution methodology for solid environmental samples and a crude pre-concentration of actinides (uranium, plutonium, thorium, americum) following the dissolution process to enable compatibility with the Automated Radionuclide Separation System-Environmental (ARSIIe) from Northstar Engineered Technologies. It was later required by the client during a subsequent meeting (August 2012, Quebec City, Quebec, Canada) that strontium be included in the list of analytes for which the sample preparation methodology should be applicable. This project was accomplished by executing a rigorous research and development strategy for soil dissolution that focuses on field deployment, efficiency, and the resulting dissolution being compatible with radiochemical separation performed by the ARSIIe using compatible designed protocols (necessary for controls and reproducibility). It was required by the client that the method of dissolution be simple (field-deployable), reliable, complete, and contained in as small a volume as possible (10- to 20-mL target). In addition, up to 1 gram of solid environmental samples needed to be solubilized through a lithium metaborate fusion technique, using the M4 Fluxer unit from Corporation Scientifique Claisse.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Observational · Consensus signal: Observational
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.582
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.017
GPT teacher head0.263
Teacher spread0.246 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designObservational
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2016
Admission routes1
Has abstractyes

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