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Record W2725396593 · doi:10.1149/ma2017-02/9/682

Pourbaix Diagrams As a Root for the Simulation of Polarization Curves for Corroding Metal Surfaces

2017· article· en· W2725396593 on OpenAlexaff
Samuel C. Perry, Janine Mauzeroll

Bibliographic record

VenueECS Meeting Abstracts · 2017
Typearticle
Languageen
FieldMaterials Science
TopicElectron and X-Ray Spectroscopy Techniques
Canadian institutionsMcGill University
Fundersnot available
KeywordsPourbaix diagramTafel equationPolarization (electrochemistry)CorrosionMetalThermodynamicsChemistryMaterials scienceMetallurgyElectrochemistryPhysical chemistryPhysicsElectrode

Abstract

fetched live from OpenAlex

The corrosion of metals is a much researched area thanks to its importance in the development of materials for a wide range of applications. A common means of experimental analysis of the corrosion rate of a specific metal is the recording of polarization curves and subsequent Tafel analysis. Comparison of such data with simulated examples provides useful validation of experimental data, as well as a better understanding of the specific reactions occurring at the metal surface. Many existing models require knowledge of parameters such as the exchange current density and Tafel slope, which requires the experiment to be conducted before the model is run. Here, we propose a model based around the Pourbaix diagram, where input parameters are either simply calculated from reaction schemes, or are easily accessible from thermodynamic data tables. In this work we use Pourbaix diagrams as a means for simulating a polarization curve at a corroding iron surface. Pourbaix diagrams show the boundaries between the changing thermodynamically stable species at a metal surface in an aqueous environment as a function of the applied potential and pH. The position of these boundaries can therefore be used to model the onset of the corresponding oxidation and reduction reactions by combining the equation of the appropriate boundary line with Butler-Volmer kinetics. At the same time, the change in pH local to the metal surface is monitored by simulating the flux of protons generated during the oxidation process, and the impact of this on the corrosion potentials and rate is taken into account. This is of great importance as the corrosion rate and the corrosion product varies according to the pH at the metal surface. In this way, we show a simple means for the simple simulation of a polarisation curve at an iron surface, which is in excellent agreement with an experimentally recorded curve under the same conditions. This same method can then be applied to more complex metal alloys such as stainless steels, by combining the Pourbaix diagrams for the appropriate alloy components. This allows the model to be used as a standalone analytical tool for the prediction of corrosion behaviour of novel alloys before they are developed, as well as for the validation of experimental data obtained from existing samples. Figure 1: Pourbaix diagram for the iron - water system Figure 1

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.003
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.005
Threshold uncertainty score0.490

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0020.003
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0010.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.029
GPT teacher head0.327
Teacher spread0.298 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations2
Published2017
Admission routes1
Has abstractyes

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