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Record W2728387575 · doi:10.1002/anie.201705197

Axially Symmetric U−O−Ln‐ and U−O−U‐Containing Molecules from the Control of Uranyl Reduction with Simple f‐Block Halides

2017· article· en· W2728387575 on OpenAlexfundno aff
Polly L. Arnold, Bradley E. Cowie, Markéta Suvova, Markus Zegke, Nicola Magnani, Éric Colineau, Jean‐Christophe Griveau, R. Caciuffo, Jason B. Love

Bibliographic record

VenueAngewandte Chemie International Edition · 2017
Typearticle
Languageen
FieldChemistry
TopicRadioactive element chemistry and processing
Canadian institutionsnot available
FundersJoint Research CentreEngineering and Physical Sciences Research CouncilNatural Sciences and Engineering Research Council of CanadaUniversity of EdinburghEuropean Commission
KeywordsHalideUranylChemistryAxial symmetryMoleculeReduction (mathematics)Simple (philosophy)Block (permutation group theory)CrystallographyPhysical chemistryInorganic chemistryPhysicsOrganic chemistryMathematicsCombinatorics

Abstract

fetched live from OpenAlex

Abstract The reduction of U VI uranyl halides or amides with simple Ln II or U III salts forms highly symmetric, linear, oxo‐bridged trinuclear U V /Ln III /U V , Ln III /U IV /Ln III , and U IV /U IV /U IV complexes or linear Ln III /U V polymers depending on the stoichiometry and solvent. The reactions can be tuned to give the products of one‐ or two‐electron uranyl reduction. The reactivity and magnetism of these compounds are discussed in the context of using a series of strongly oxo‐coupled homo‐ and heterometallic poly(f‐block) chains to better understand fundamental electronic structure in the f‐block.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.029
Threshold uncertainty score0.471

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.015
GPT teacher head0.256
Teacher spread0.241 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations37
Published2017
Admission routes1
Has abstractyes

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