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Record W2744868093 · doi:10.1002/ejoc.201701044

Vibrational Circular Dichroism Unveils Chiroptical, Electrical, and Magnetic Properties of Borylated Isocyanides and Aldehydes

2017· article· en· W2744868093 on OpenAlexaff
Giuseppe Mazzeo, Giovanna Longhi, Victoria B. Corless, Adam Zajdlik, Andrei K. Yudin, Sergio Abbate

Bibliographic record

VenueEuropean Journal of Organic Chemistry · 2017
Typearticle
Languageen
FieldChemistry
TopicMolecular spectroscopy and chirality
Canadian institutionsUniversity of Toronto
FundersUniversità degli Studi di BresciaFondazione Cariplo
KeywordsChemistryVibrational circular dichroismCircular dichroismMagnetic circular dichroismAbsolute configurationAbsorption (acoustics)Absorption spectroscopyCrystallographyComputational chemistryPhotochemistryStereochemistrySpectral lineOptics

Abstract

fetched live from OpenAlex

The absolute configurations of two novel chiral borylated compounds bearing the ( S )‐proline‐derived N ‐carboxymethylproline ligand have been studied by vibrational circular dichroism (VCD) in conjunction with IR absorption, UV absorption, and electronic circular dichroism (ECD). DFT and time‐dependent DFT calculations allowed us to interpret the observed spectra and gave credibility to the VCD data. The VCD data in the CH stretching region were also considered. The experimental and computational data are consistent with those obtained by NMR spectroscopy. The investigation of the C=O stretching region should assist in the future assignment of the absolute configuration of chiral borylated compounds bearing carbonyl groups.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.009
Threshold uncertainty score0.815

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.010
GPT teacher head0.208
Teacher spread0.198 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2017
Admission routes1
Has abstractyes

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