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Record W2747801490 · doi:10.1021/acs.jpcc.7b02944

Elucidating the Importance of Pore Structure in Determining the Double-Layer Capacitance of Nanoporous Carbon Materials

2017· article· en· W2747801490 on OpenAlexafffund
Jocelyn E. Zuliani, Charles Q. Jia, Donald W. Kirk

Bibliographic record

VenueThe Journal of Physical Chemistry C · 2017
Typearticle
Languageen
FieldMaterials Science
TopicSupercapacitor Materials and Fabrication
Canadian institutionsUniversity of Toronto
FundersNatural Sciences and Engineering Research Council of CanadaNational Natural Science Foundation of China
KeywordsNanoporousMaterials scienceCapacitanceCarbon fibersSupercapacitorNanotechnologyScanning electron microscopePorosityElectrolyteNanostructureAdsorptionChemical engineeringCarbide-derived carbonElectrodeComposite materialChemistryCarbon nanotube

Abstract

fetched live from OpenAlex

Porous carbon is a common electrode material used in electrochemical double-layer capacitors, in which energy is stored by physical adsorption of electrolyte ions on the carbon’s surface, forming an electrical double layer (EDL). However, due to the complex nanoporous network of carbon materials, it is difficult to characterize the EDL structure. This work demonstrates that the understanding of the EDL structure in nanoporous carbon materials can be improved by defining the pore shapes using ultrahigh resolution scanning electron microscopy (SEM). The SEM images reveal a continuous network of curved pores. This characterization, along with the experimentally determined surface areas and pore sizes, enabled the investigation of the applicability of various models describing the EDL configuration. This study found that, by using the microscopic information to characterize the 3-D nanostructure and select the appropriate models for the pore shape, it is possible to predict a porous carbon material’s experimental capacitance within ±8%. This updated approach may be used to identify ideal pore structures and top-performing carbon materials. It is clear that using ultrahigh resolution SEM images to understand the relationship between pore shape, EDL structure, and capacitance provides valuable insight into the complexity of energy storage in nanoporous carbon materials.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.002
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.002
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.022
GPT teacher head0.270
Teacher spread0.248 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations14
Published2017
Admission routes2
Has abstractyes

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