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Record W2760894607 · doi:10.1021/acs.chemmater.7b04015

Tl<sub>2</sub>Ag<sub>12</sub>Se<sub>7</sub>: A New pnp Conduction Switching Material with Extraordinarily Low Thermal Conductivity

2017· article· en· W2760894607 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueChemistry of Materials · 2017
Typearticle
Languageen
FieldMaterials Science
TopicCrystal Structures and Properties
Canadian institutionsUniversity of Waterloo
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsSelenideSeebeck coefficientThalliumThermal conductionStoichiometryMaterials scienceElectrical resistivity and conductivityThermoelectric effectType (biology)SemiconductorThermoelectric materialsThermal conductivityBand gapConductivityCrystallographySeleniumAnalytical Chemistry (journal)Condensed matter physicsChemistryOptoelectronicsPhysicsPhysical chemistryThermodynamics

Abstract

fetched live from OpenAlex

While continuing our investigations of thallium chalcogenides because of their outstanding thermoelectric properties, we discovered a new selenide with an interesting pnp switching behavior around 400 K. Tl 2 Ag 12 Se 7 was prepared via high temperature reaction from the elements in the stoichiometric ratio. This selenide crystallizes in a new structure type, namely a √3 × √3 × 1 super cell of the Zr 2 Fe 12 P 7 type, adopting space group P 3̅, a = b = 18.9153(18) Å, c = 4.3783(4) Å, and V = 1356.6(2) Å 3 ( Z = 3). The structure consists of a complex network of three-dimensionally connected AgSe 4 tetrahedra that include linear channels filled with thallium atoms. This material is a semiconductor with an experimentally derived activation gap of 0.8 eV and extraordinarily low thermal conductivity of <0.45 W m –1 K –1 . A reversible phase transition causes a pnp switch from p-type to n-type and back to p-type conduction beginning around 390 K, with the thermopower changing fast from +230 μV K –1 at 390 K to −230 μV K –1 at 410 K, and then back up to +75 μV K –1 at 420 K.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Scholarly communication, Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0010.001
Scholarly communication0.0010.001
Open science0.0010.001
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.022
GPT teacher head0.234
Teacher spread0.212 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it