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Record W2766239109 · doi:10.1021/acs.jpca.7b08984

Rotational Spectroscopy of <i>p</i>-Toluic Acid and Its 1:1 Complex with Water

2017· article· en· W2766239109 on OpenAlex
Elijah G. Schnitzler, Nathan A. Seifert, Ignes Kusuma, Wolfgang Jäger

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueThe Journal of Physical Chemistry A · 2017
Typearticle
Languageen
FieldChemistry
TopicMolecular Spectroscopy and Structure
Canadian institutionsUniversity of Alberta
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsSpectroscopyChemistryMaterials sciencePhysicsNuclear magnetic resonanceQuantum mechanics

Abstract

fetched live from OpenAlex

The structure and internal dynamics of p -toluic acid and its 1:1 complex with water were investigated in the gas phase using chirped-pulse and cavity-based Fourier transform microwave spectroscopy. One conformer and one isomer were identified for the monomer and monohydrate, respectively. In the monohydrate, water acts as both a hydrogen bond donor and acceptor, participating in a six-membered intermolecular ring with the carboxyl group. Both a - and b -type transitions were observed for the monomer; only a -type transitions were observed for the monohydrate. Rotational transitions of both species show splittings originating from methyl internal rotation, for which the potentials include 3- and 6-fold symmetry terms of similar amplitude. For the monomer, a few b -type transitions are missing, and their intensities were found to be transferred to c -type transitions with common energy levels, which are otherwise forbidden. No splittings attributable to a water internal tunneling motion were observed for the monohydrate. Furthermore, the absence of c -type transitions in the spectrum of the monohydrate, despite the large μ c dipole moment component of the equilibrium geometry obtained by ab initio calculations, is consistent with a barrierless wagging motion of the free hydrogen of water, leading to an average μ c dipole moment component of zero. These results provide insights regarding the interactions between atmospheric p -toluic acid and water in prenucleation complexes and at the air–water interface of aqueous aerosols, where p -toluic acid may act as a surfactant.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score0.354

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.257
Teacher spread0.247 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it