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Record W2766849915 · doi:10.1021/acs.jpcc.7b08691

Evaluation of Surface-Enhanced Raman Spectroscopy Substrates from Single-Molecule Statistics

2017· article· en· W2766849915 on OpenAlexafffund
Evan Kiefl, R. F. Kiefl, Diego P. dos Santos, Alexandre G. Brolo

Bibliographic record

VenueThe Journal of Physical Chemistry C · 2017
Typearticle
Languageen
FieldMaterials Science
TopicGold and Silver Nanoparticles Synthesis and Applications
Canadian institutionsUniversity of British ColumbiaUniversity of Victoria
FundersBritish Columbia Knowledge Development FundNatural Sciences and Engineering Research Council of CanadaConselho Nacional de Desenvolvimento Científico e Tecnológico
KeywordsRaman spectroscopySurface-enhanced Raman spectroscopyMoleculeMaterials scienceSpectroscopySurface (topology)Analytical Chemistry (journal)Molecular physicsStatisticsChemistryRaman scatteringOpticsPhysicsMathematicsEnvironmental chemistryQuantum mechanicsGeometryOrganic chemistry

Abstract

fetched live from OpenAlex

Accurate quantification of substrate characteristics is a central pursuit within the field of surface-enhanced Raman spectroscopy (SERS). A theory based on single-molecule SERS (SM-SERS) statistics was developed for comprehensive substrate evaluation. This approach is applicable to general substrates possessing many hotspots and is capable of quantifying hotspot strength variation using a minimal set of fitting parameters. The model was validated for simulated substrates and then applied to the SM-SERS statistics of a roughened silver electrode, for which the degree of hotspot uniformity was quantified. The fitted model parameters provide important information concerning the structure–activity relationship of hotspots and can be used to directly compare SERS substrates. Overall, our results present an experimentally determinable parameter set that potentially improves upon the widely used “average enhancement factor” metric currently used for SERS substrate evaluation.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.003
metaresearch head score (Gemma)0.008
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.016

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0030.008
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0010.001
Science and technology studies0.0000.001
Scholarly communication0.0010.001
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.035
GPT teacher head0.304
Teacher spread0.269 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations13
Published2017
Admission routes2
Has abstractyes

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Same venueThe Journal of Physical Chemistry CSame topicGold and Silver Nanoparticles Synthesis and ApplicationsFrench-language works237,207