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Record W2769749548 · doi:10.1021/acschembio.7b00996

Determinants and Prediction of Esterase Substrate Promiscuity Patterns

2017· article· en· W2769749548 on OpenAlexafffund
Mónica Martínez‐Martínez, Cristina Coscolín, Gerard Santiago, Jennifer Chow, P.J. Stogios, Rafael Bargiela, Christoph Gertler, José Navarro‐Fernández, Alexander Bollinger, Stephan Thies, Celia Méndez–García, Ana Popovic, Greg Brown, Tatyana N. Chernikova, Antonio García‐Moyano, Gro Elin Kjæreng Bjerga, Pablo Pérez-García, Trần Ngọc Hải, Mercedes V. del Pozo, Runar Stokke, Ida Helene Steen, Hong Cui, Xiaohui Xu, B. Nocek, María M. Alcaide, Marco A. Distaso, Victoria Mesa, Ana I. Peláez, Jesús Sánchez, Patrick C. F. Buchholz, Jürgen Pleiss, Antonio Fernàndez-Guerra, Frank Oliver Glöckner, Olga V. Golyshina, Michail M. Yakimov, Alexei Savchenko, Karl‐Erich Jaeger, Alexander F. Yakunin, Wolfgang R. Streit, Peter N. Golyshin, Vı́ctor Guallar, Manuel Ferrer, The INMARE Consortium

Bibliographic record

VenueACS Chemical Biology · 2017
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicEnzyme Catalysis and Immobilization
Canadian institutionsUniversity of Toronto
FundersH2020 Societal ChallengesBiotechnology and Biological Sciences Research CouncilNatural Sciences and Engineering Research Council of CanadaMinisterio de Economía y CompetitividadGenome CanadaEuropean Regional Development FundDeutsche ForschungsgemeinschaftFP7 Food, Agriculture and Fisheries, BiotechnologyDepartamento Administrativo de Ciencia, Tecnología e Innovación (COLCIENCIAS)
KeywordsSubstrate (aquarium)Active siteSasaCatalytic triadDehalogenaseComputational biologyBiologyChemistryBiological systemEnzymeBiochemistryEcology

Abstract

fetched live from OpenAlex

Esterases receive special attention because of their wide distribution in biological systems and environments and their importance for physiology and chemical synthesis. The prediction of esterases' substrate promiscuity level from sequence data and the molecular reasons why certain such enzymes are more promiscuous than others remain to be elucidated. This limits the surveillance of the sequence space for esterases potentially leading to new versatile biocatalysts and new insights into their role in cellular function. Here, we performed an extensive analysis of the substrate spectra of 145 phylogenetically and environmentally diverse microbial esterases, when tested with 96 diverse esters. We determined the primary factors shaping their substrate range by analyzing substrate range patterns in combination with structural analysis and protein-ligand simulations. We found a structural parameter that helps rank (classify) the promiscuity level of esterases from sequence data at 94% accuracy. This parameter, the active site effective volume, exemplifies the topology of the catalytic environment by measuring the active site cavity volume corrected by the relative solvent accessible surface area (SASA) of the catalytic triad. Sequences encoding esterases with active site effective volumes (cavity volume/SASA) above a threshold show greater substrate spectra, which can be further extended in combination with phylogenetic data. This measure provides also a valuable tool for interrogating substrates capable of being converted. This measure, found to be transferred to phosphatases of the haloalkanoic acid dehalogenase superfamily and possibly other enzymatic systems, represents a powerful tool for low-cost bioprospecting for esterases with broad substrate ranges, in large scale sequence data sets.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.003
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.006

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.003
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.001
Bibliometrics0.0020.001
Science and technology studies0.0000.000
Scholarly communication0.0010.001
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.015
GPT teacher head0.271
Teacher spread0.256 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations147
Published2017
Admission routes2
Has abstractyes

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