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Record W2790239671 · doi:10.1002/cssc.201800049

Tunable Bifunctional Activity of Mn<sub><i>x</i></sub>Co<sub>3−<i>x</i></sub>O<sub>4</sub> Nanocrystals Decorated on Carbon Nanotubes for Oxygen Electrocatalysis

2018· article· en· W2790239671 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueChemSusChem · 2018
Typearticle
Languageen
FieldEnergy
TopicElectrocatalysts for Energy Conversion
Canadian institutionsDalhousie UniversityCanadian Light Source (Canada)
FundersArgonne National LaboratoryOffice of ScienceCanadian Light SourceEngineering and Physical Sciences Research CouncilChina Scholarship CouncilU.S. Department of Energy
KeywordsElectrocatalystOxygen evolutionCatalysisMaterials scienceBifunctionalElectrochemistryNanocrystalline materialCobaltNanocrystalOxideChemical engineeringOxygenMetalNanotechnologyInorganic chemistryChemistryPhysical chemistryElectrodeMetallurgy

Abstract

fetched live from OpenAlex

Abstract Noble‐metal‐free electrocatalysts are attractive for cathodic oxygen catalysis in alkaline membrane fuel cells, metal–air batteries, and electrolyzers. However, much of the structure–activity relationship is poorly understood. Herein, the comprehensive development of manganese cobalt oxide/nitrogen‐doped multiwalled carbon nanotube hybrids (Mn x Co 3− x O 4 @NCNTs) is reported for highly reversible oxygen reduction and evolution reactions (ORR and OER, respectively). The hybrid structures are rationally designed by fine control of surface chemistry and synthesis conditions, including tuning of functional groups at surfaces, congruent growth of nanocrystals with controllable phases and particle sizes, and ensuring strong coupling across catalyst–support interfaces. Electrochemical tests reveal distinctly different oxygen catalytic activities among the hybrids, Mn x Co 3− x O 4 @NCNTs. Nanocrystalline MnCo 2 O 4 @NCNTs (MCO@NCNTs) hybrids show superior ORR activity, with a favorable potential to reach 3 mA cm −2 and a high current density response, equivalent to that of the commercial Pt/C standard. Moreover, the hybrid structure exhibits tunable and durable catalytic activities for both ORR and OER, with a lowest overall potential of 0.93 V. It is clear that the long‐term electrochemical activities can be ensured by rational design of hybrid structures from the nanoscale.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesMeta-epidemiology (narrow)
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.013
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0020.001
Bibliometrics0.0010.002
Science and technology studies0.0010.001
Scholarly communication0.0000.001
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.222
Teacher spread0.211 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it