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Recovery of Zn from Unsorted Spent Batteries Using Solvent Extraction and Electrodeposition

2018· article· en· W2790577062 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueJournal of Environmental Engineering · 2018
Typearticle
Languageen
FieldEngineering
TopicExtraction and Separation Processes
Canadian institutionsInstitut National de la Recherche Scientifique
Fundersnot available
KeywordsLeaching (pedology)Sulfuric acidAqueous solutionExtraction (chemistry)ChemistryZincSolventAqueous two-phase systemKeroseneNuclear chemistryPrecipitationStripping (fiber)Inorganic chemistryChromatographyMaterials scienceOrganic chemistry

Abstract

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This study focused on the selective recovery of zinc (Zn) from a leaching solution emerging from a sulfuric acid leaching process applied to unsorted spent batteries. Precipitation and solvent extraction were investigated. According to the results, solvent extraction using Cyanex 272 allowed for the selective removal of Zn from the solution containing high amounts of metals (∼19.4 g Zn/L, ∼23.4 g Mn/L, ∼3.27 g Cd/L, ∼3.19 g Ni/L, and ∼0.25 g Co/L). According to the results, the solvent extraction process was capable of recovering 97.6% of Zn from this leaching solution under the following conditions: two stages of extraction in the presence of an organic solution made of Cyanex 272 (30%, v/v) and tributylphosphate (TBP—2%, v/v) in kerosene, pH=2.2, organic/aqueous (O/A) ratio = 2/1, and T=50°C. The Zn present in the organic phase was then stripped using 0.4 M H2SO4 with an O/A ratio fixed at 2/1. This stripping step allowed for the recovery of 81.8% of the Zn initially present in the organic phase. Subsequently, 82.4% of the Zn stripped in the aqueous solution was then electrically deposited after 3 h at pH=2 with a current density fixed at 360 A/m2.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.076
Threshold uncertainty score0.380

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.211
Teacher spread0.203 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it