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Record W2791823117 · doi:10.3934/environsci.2018.2.67

Fluorescence Detection of Zinc Oxide Nanoparticles in Water Contamination Analysis based on Surface Reactivity with Porphyrin

2018· article· en· W2791823117 on OpenAlexaff
Wenyu Zhang, Edward P. C. Lai

Bibliographic record

VenueAIMS environmental science · 2018
Typearticle
Languageen
FieldMaterials Science
TopicAdvanced Nanomaterials in Catalysis
Canadian institutionsCarleton University
Fundersnot available
KeywordsPorphyrinFluorophoreNanoparticleFluorescenceQuenching (fluorescence)ZincAqueous solutionAnalytical Chemistry (journal)Materials scienceContaminationChemistryPhotochemistryNanotechnologyChromatographyOpticsOrganic chemistry

Abstract

fetched live from OpenAlex

A simple rapid analytical method for determining the concentration of ZnO nanoparticles in aqueous dispersion has been developed by adding porphyrin (TCPP) as a fluorophore into the water sample for fluorescence analysis. Quenching of the emission intensity at 650 nm provides a Stern-Volmer plot with adequate sensitivity for the detection of ZnO nanoparticles from 0.15 mg/mL up to 1.5 mg/mL. A new emission peak at 605 nm can be attributed to the formation of a unique ZnO-TCPP complex. This unique emission peak is good for both identification and quantitation of ZnO nanoparticles at low concentrations down to 0.0015 mg/mL. The new method affords a linear dynamic range up to 1.2 mg/mL.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.200
Threshold uncertainty score0.627

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.002
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.216
Teacher spread0.210 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations12
Published2018
Admission routes1
Has abstractyes

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