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Record W2888086341 · doi:10.1016/j.trac.2018.08.004

Analytical characterization of N-halogenated peptides produced by disinfection: Formation, degradation, and occurrence in water

2018· article· en· W2888086341 on OpenAlexafffund
Ping Jiang, Lindsay K. Jmaiff Blackstock, Nicholas J. P. Wawryk, Guang Huang, Xing‐Fang Li

Bibliographic record

VenueTrAC Trends in Analytical Chemistry · 2018
Typearticle
Languageen
FieldEnvironmental Science
TopicWater Treatment and Disinfection
Canadian institutionsUniversity of Alberta
FundersNatural Sciences and Engineering Research Council of CanadaUniversity of Alberta
KeywordsDegradation (telecommunications)Characterization (materials science)Environmental chemistryChemistryEnvironmental scienceMaterials scienceNanotechnologyEngineering

Abstract

fetched live from OpenAlex

Organic N -haloamines are water disinfection byproducts resulting from reactions between dissolved organic nitrogen and disinfectants . N -halogenated peptides, an important group of organic N -haloamines, have been overlooked over the past. In this review, we highlight peptides as the precursors for N -halogenated peptides during wastewater and drinking water disinfection. We discuss the analysis of N -halogenated peptides using methods based on titration , spectrophotometry , chromatography , and advanced liquid chromatography–mass spectrometry and the studies of the formation, degradation, and occurrence of N -halogenated peptides in water. While each method contributes to the evaluation of mechanisms and kinetics of formation and degradation of N -halogenated peptides in laboratory solution, only the development of highly sensitive and selective mass spectrometric methods enables the detection of trace levels of N -halogenated peptides in authentic disinfected water samples. Overall, reactions between peptides and disinfectants take place in milliseconds through an electrophilic substitution process. The N -halogenated peptides formed are relatively stable, leading to their sustainability in disinfected water. The recent detection of N -chlorinated peptides as disinfection byproducts using liquid chromatography–mass spectrometry in drinking water brings attention to these compounds. Further investigation of N -halogenated peptides on their occurrence and toxicological impacts are required to evaluate their health relevance.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.194
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.012
GPT teacher head0.246
Teacher spread0.234 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations21
Published2018
Admission routes2
Has abstractyes

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