Overcoming the Hurdle from Undergraduate Lab to Research Lab: A Guided-Inquiry Structural Characterization of a Complex Mixture in the Upper-Division Undergraduate Organic Lab
Why this work is in the frame
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Bibliographic record
Abstract
This guided-inquiry, upper-division undergraduate organic lab experiment, a hybrid of problem-based learning (PBL); process-oriented, guided-inquiry learning (POGIL); and peer-led team learning (PLTL) has been developed to ease the transition from the undergraduate lab to a research lab environment. The characterization of a mixture of camphor and p-coumaric acid involves a complex separation as well as thoughtful NMR experiments and solvent selection. Technique and problem-solving instruction (involving thin-layer and column chromatography as well as 1D [coupling constant analysis] and 2D [COSY, HSQC, and HMBC] NMR spectroscopy) has been simplified for the instructor by the development of videos, detailed notes, and assignment worksheets.
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Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.001 | 0.002 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.000 | 0.000 |
| Bibliometrics | 0.000 | 0.001 |
| Science and technology studies | 0.000 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.001 | 0.000 |
| Research integrity | 0.000 | 0.001 |
| Insufficient payload (model declined to judge) | 0.000 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it