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Record W2899189938

Understanding long-range transport mechanisms of perfluoroalkyl substances

2017· dissertation· en· W2899189938 on OpenAlexaboutno aff
Heidi M. Pickard

Bibliographic record

VenueMemorial University Research Repository (Memorial University) · 2017
Typedissertation
Languageen
FieldEnvironmental Science
TopicPer- and polyfluoroalkyl substances research
Canadian institutionsnot available
Fundersnot available
KeywordsDeposition (geology)Environmental chemistryChlorofluorocarbonIce coreEnvironmental scienceAtmosphere (unit)PollutantSedimentary depositional environmentChemistryMeteorologyGeologyGeographyClimatologyOrganic chemistryGeomorphology
DOInot available

Abstract

fetched live from OpenAlex

Perfluoroalkyl acids (PFAAs) are persistent, bioaccumulative compounds found
\nubiquitously within the environment. They can be formed from the atmospheric oxidation
\nof volatile precursor compounds and undergo long-range transport (LRT) through the
\natmosphere and ocean to remote locations. Ice caps preserve a temporal record of PFAA
\ndeposition making them useful in studying the atmospheric trends in LRT of PFAAs as
\nwell as understanding major pollutant sources and production changes over time.
\nA 15 m ice core representing 38 years of deposition (1977 – 2015) was collected
\nfrom the Devon Ice Cap in Nunavut and analyzed for PFAAs. Samples were concentrated
\nby solid phase extraction and analyzed by UPLC-MS/MS, IC, and ICP-OES. Both shortand
\nlong-chain perfluorocarboxylic acids (PFCAs) and perfluorosulfonic acids (PFSAs)
\nwere detected in the samples, with fluxes ranging from <LOD to 4.44×10⁴ ng m ⁻² yr⁻¹.
\nIn this work I assess temporal trends in deposition, homologue profiles, ion
\ntracers, air mass transport models, and production and regulation trends to characterize
\nthe PFAA depositional profile on the Devon Ice Cap and to further understand the LRT
\nmechanisms of these persistent pollutants. In Chapter 3 my results demonstrate that the
\nPFCAs and perflurooctane sulfonate (PFOS) have continuous and increasing deposition
\non Devon Ice Cap, despite recent North American regulations and phase-outs. I propose
\nthat this is the result of on-going emission and use of these compounds, their precursors
\nand other newly unidentified compounds in regions outside of North America. Through
\nmodelling air mass transport densities, and comparing temporal trends in deposition with production changes of possible sources, I find that Eurasian sources, particularly from
\nContinental Asia are large contributors to the global pollutants impacting Devon Ice Cap.
\nBy comparing PFAAs to their precursors and correlating pairs of PFCAs, I determine that
\ndeposition of PFAAs is dominated by atmospheric formation from volatile precursor
\nsources, and major ion analysis provides new information regarding the transport of
\nPFAAs, confirming that marine aerosol inputs are unimportant to the LRT mechanisms of
\nthese compounds. In Chapter 4 my results from the Arctic ice core analysis show a tenfold
\nincrease in short-chain PFCA (scPFCA) deposition between 1986 and 2014, which
\ncoincides with increased production and atmospheric burden of chlorofluorocarbon (CFC)-
\nreplacement compounds. This is the first multi-decadal temporal record of scPFCA
\ndeposition and indicates that Montreal Protocol-mandated introduction of CFC-replacement
\ncompounds for the heat-transfer industry is the dominant source of scPFCAs to remote
\nregions.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Science and technology studies, Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Not applicable · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.574
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0020.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0010.002
Science and technology studies0.0030.002
Scholarly communication0.0000.002
Open science0.0040.000
Research integrity0.0010.002
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.067
GPT teacher head0.281
Teacher spread0.215 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designNot applicable
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2017
Admission routes1
Has abstractyes

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