MétaCan
Menu
Back to cohort
Record W2907384529 · doi:10.1021/acsami.8b15946

Design Strategy for the Controlled Generation of Cationic Frameworks and Ensuing Anion-Exchange Capabilities

2018· article· en· W2907384529 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueACS Applied Materials & Interfaces · 2018
Typearticle
Languageen
FieldMaterials Science
TopicCovalent Organic Framework Applications
Canadian institutionsUniversity of CalgaryUniversity of Ottawa
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsMaterials scienceIon exchangeCationic polymerizationSystems engineeringNanotechnologyIonProcess engineeringEngineeringOrganic chemistryPolymer chemistry

Abstract

fetched live from OpenAlex

Cationic frameworks are an emerging class of exceptional solid adsorbents capable of encapsulating highly toxic and persistent anionic pollutants. The controlled generation of cationic frameworks, however, lags behind the abundant design strategies devised to control the structures and topologies of neutral frameworks. In this regard, we report a rational approach that allows the conversion of the synthetic approach toward constructing a neutral framework into one allowing for the synthesis of a cationic one without incurring any changes to the overall topology or the selected metal ion. We demonstrate that the replacement of a functional group on an organic linker that promotes a similar coordination mode, but bearing one less negative charge, can yield the systematic generation of cationic frameworks. Moreover, we confirm the cationic nature of the metal-organic frameworks through preliminary anion-exchange experiments and propose a method to retain permanent porosity in cationic frameworks through the use of strongly binding anions. Altogether, these results show great promise for the construction of tunable nanoporous frameworks capable of carrying out anion-exchange processes.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.047
Threshold uncertainty score0.921

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.049
GPT teacher head0.289
Teacher spread0.240 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it