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Record W2908555518 · doi:10.1002/apj.2285

Insights into the integrated effects of polymeric pretreatment and catalytic hydrotreatment of light gas oil

2019· article· en· W2908555518 on OpenAlexafffund
Abidemi Olomola, Prachee Misra, J.M. Chitanda, Ajay K. Dalai, John Adjaye

Bibliographic record

VenueAsia-Pacific Journal of Chemical Engineering · 2019
Typearticle
Languageen
FieldEngineering
TopicCatalysis and Hydrodesulfurization Studies
Canadian institutionsSyncrude (Canada)University of Saskatchewan
FundersMitacsSyncrude
KeywordsHydrodesulfurizationChemistryGlycidyl methacrylateCatalysisFlue-gas desulfurizationPolymerAdsorptionNitrogenChemical engineeringOrganic chemistrySulfurFuel oilCopolymerWaste management

Abstract

fetched live from OpenAlex

Abstract A study has been carried out in detail to measure the effects of the removal of nitrogen compounds on the hydrotreatment of light gas oil (LGO) using a synthesized polymer consisting of a polymer support, copolymer of glycidyl methacrylate and ethylene glycol dimethacrylate (PGMA‐co‐EDGMA), a π‐acceptor moiety (2,4,5,7‐tetranitrofluorenone, TENF), and a three‐carbon linker (diaminopropane, DAP (3)). The primary focus of this paper is first to study the effects of selectively removing nitrogen compounds on the hydrotreatment of LGOs. Removal of these catalyst inhibiting and poisoning compounds prior to hydrotreatment will help in improving the hydroprocessing efficiency as well as in reducing the chemical fouling, thus improving the catalyst life. Second, the effectiveness on the reusability of bulk polymer after regeneration was studied. To achieve this, nitrogen compounds from LGO were adsorbed on the synthesized polymer by mixing polymer and LGO. The polymer was regenerated by washing with toluene in a Soxhlet apparatus. Hydrotreating experiments were performed in a pilot scale trickle‐bed reactor. To create a baseline for monitoring the hydrotreatment activity, untreated LGO (without polymer adsorption) was hydrotreated with a commercial NiMo/γ‐Al 2 O 3 catalyst and analyzed for nitrogen, sulfur, and aromatics content. The pretreated feed (with polymer adsorption) was also hydrotreated, and the results were compared. The results show that prior selective removal of nitrogen compounds improved overall hydrotreatment activity and resulted in additional decrease of 18.7%, 8.3%, and 9.4% in total nitrogen, sulfur, and aromatics content, respectively.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.012
Threshold uncertainty score0.527

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.002
GPT teacher head0.165
Teacher spread0.163 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations2
Published2019
Admission routes2
Has abstractyes

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