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Optimization of Flow Injection (FI) – Spectrophotometry for Hydroquinone Analysis

2019· article· en· W2911814383 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

aboutThe title or abstract carries a Canadian signal from the geographic lexicon.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueThe Journal of Pure and Applied Chemistry Research · 2019
Typearticle
Languageen
FieldChemistry
TopicDye analysis and toxicity
Canadian institutionsnot available
Fundersnot available
KeywordsHydroquinonePhloroglucinolChemistrySpectrophotometryChromatographyNuclear chemistryOrganic chemistry

Abstract

fetched live from OpenAlex

Hydroquinone is one of the phenolic compounds used in various cosmetic products for skin lightening as it can inhibit tyrosinase enzyme in producing melanin. However, hydroquinone is classified as a toxic compound, therefore, several countries such as Africa, Canada, and Indonesia prohibits hydroquinone usage in cosmetics. This research was focused on the development of a method for hydroquinone analysis using flow injection (FI) combined with spectrophotometry based on the reaction of hydroquinone with phloroglucinol in alkaline condition producing orange complex detected at 493 nm. The FI method was optimized based on operational factors and chemical factors in order to achieve sensitivity. The maximum sensitivity of FI method was achieved under operational condition of 100 μL sample volume, 100 cm mixing coil 1, 50 cm mixing coil 2 and 2.8 mL/min with the chemical condition of 0.005 mol/L NaOH and 0.001 mol/L phloroglucinol. Under these optimum conditions, the proposed method showed linearity in the range concentration of 2 – 80 mg/L and the method was applied to cosmetic sample with acceptable recovery

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.035
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0020.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.020
GPT teacher head0.300
Teacher spread0.280 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it