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Record W2919824805 · doi:10.22215/etd/2019-13448

Corrosion Behaviour of High-Carbon High-Molybdenum Stellite Alloys in Amine Environment

2019· dissertation· en· W2919824805 on OpenAlexaff
Kafeel Kamal

Bibliographic record

Venuenot available
Typedissertation
Languageen
FieldEngineering
TopicHigh-Temperature Coating Behaviors
Canadian institutionsCarleton University
Fundersnot available
KeywordsStelliteHardfacingMetallurgyMaterials scienceCorrosionMolybdenumCarbideMicrostructure

Abstract

fetched live from OpenAlex

Stellite alloys are cobalt-based alloys which display exceptional mechanical properties, wear and corrosion resistance owing to its unique chemical compositions. Stellite 6 is the most popular Stellite alloy employed in various applications, one of which is the hardfacing of valve trim components within control valves in boiler feedwater treatment systems where hydrazine and/or amine derivatives are used. Erosion-corrosion caused failure of Stellite 6 hardfacing has been reported from industry in such applications. To find a better replacement of Stellite 6 for improved corrosion resistance in amine environment, 700 series Stellite alloys, including Stellite 706, Stellite 712 and Stellite 720, are proposed, which are high-carbon high-molybdenum Stellite alloys. The corrosion performance of these alloys in morpholine solution with pH 9.5, which simulates the corrosive environment of boiler feedwater service, is evaluated using a series of electrochemical tests such as electrochemical impedance spectroscopy (EIS), potentiodynamic polarization and potentiostatic polarization. Both regular polarization tests (potential up to 1.2 V) and failure polarization tests (potential up to 12 V) are conducted on the alloys. The former identifies general and localized corrosion behaviour, while the latter intends to fail the alloy surface to analyze their limitations. Two different surface conditions (intact and damaged) and two different temperature variables (25C and 50C) are also studied to simulate erosion-corrosion behaviour. Stellite 6 alloy is also tested under the same condition for comparison. It is shown that these 700 series Stellite alloys are comparably better than Stellite 6 with respect to oxide film stability, all exhibiting excellent corrosion resistance in morpholine solution with pH 9.5. The protective chromium oxide film on their surfaces is retained well for both regular and failure tests. These alloys behave similarly, however, Stellite 720 containing the highest carbon and molybdenum contents performed better at room temperature and Stellite 706 with the least carbon and molybdenum iii contents performed better at the elevated temperature. Although wear changes the surface condition, the corrosion resistance of the worn alloys is similar to that of intact alloys in the tested solution. The outcomes of this research suggest that 700 series Stellite alloys are good candidates for replacing Stellite 6, where Stellite 720 displayed the best performance under the conditions tested.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.261
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.005
GPT teacher head0.202
Teacher spread0.197 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2019
Admission routes1
Has abstractyes

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