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Record W2924489037 · doi:10.22215/etd/2017-12114

Electrochemical Study of Corrosion Behavior of Stellite 6 Alloy and 17-4PH Stainless Steel in Amine Solutions

2017· dissertation· en· W2924489037 on OpenAlexaff
Yi Li

Bibliographic record

Venuenot available
Typedissertation
Languageen
FieldMaterials Science
TopicCorrosion Behavior and Inhibition
Canadian institutionsCarleton University
Fundersnot available
KeywordsStelliteMaterials scienceCorrosionMetallurgyAlloyOxidePitting corrosion

Abstract

fetched live from OpenAlex

Stellite 6 alloy has been popularly employed as the material for the seat face of various control valves due to its excellent combined mechanical, corrosion, wear, and high temperature properties.However, a suggestion was made in an article that Stellite 6 alloy should be avoided in the amine containing feed water service of power plants, and Stellite 6 alloy should be replaced by stainless steels, such as 17-4PH stainless steel.To provide the power generation industry with scientific evidence, the corrosion behavior of Stellite 6 alloy and 17-4PH stainless steel is studied in morpholine solution, cyclohexylamine solution and sodium hydroxide solution at the same pH around 9.5 using electrochemical test methods such as potentiodynamic polarization, cyclic polarization, and electrochemical impedance spectroscopy (EIS) in this research.The microstructures of the tested materials and corroded surfaces are analyzed using scanning electron microscopy (SEM) with energy dispersive X-ray (EDX) spectroscopy.The experimental results show that Stellite 6 alloy and 17-4PH stainless steel are generally resistant to corrosion in amine solutions by forming a Cr-rich oxide films on their surfaces, but they can be corroded when the oxide film is broken, leading to damage of the surfaces and the removal of the materials.The oxide film of 17-4PH stainless steel is more resistant to electron transferring than that of Stellite 6 alloy, thus has better resistance to corrosion.However, the oxide film of 17-4PH stainless steel has less durability and it works well only within a certain potential range.Otherwise, Stellite 6 alloy has better overall corrosion and pitting corrosion resistance than 17-4PH stainless steel in amine environments.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.027
GPT teacher head0.304
Teacher spread0.278 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations2
Published2017
Admission routes1
Has abstractyes

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