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Record W2931645211 · doi:10.1149/ma2018-02/49/1712

Surface Ligands As Atomic Valves for Growth of Nanocrystal Quantum Dots

2018· article· en· W2931645211 on OpenAlexaff
Doh C. Lee

Bibliographic record

VenueECS Meeting Abstracts · 2018
Typearticle
Languageen
FieldMaterials Science
TopicQuantum Dots Synthesis And Properties
Canadian institutionsKootenay Association for Science & Technology
Fundersnot available
KeywordsNanorodQuantum dotNanocrystalDispersityNucleationColloidMaterials scienceContext (archaeology)NanotechnologyReactivity (psychology)Ligand (biochemistry)Chemical engineeringChemistryChemical physicsPhysical chemistryOrganic chemistryPolymer chemistry

Abstract

fetched live from OpenAlex

Growth of monodisperse quantum dots (QDs) is a pressing requirement in the context of commercial application as well as academic study, as the size uniformity is directly related to color purity in display products which have been commercialized. In the growth, surface ligands serve not only as a protection layer for QD surface but also controller for reaction kinetics. I will present our recent findings pertaining to these issues on the basis of different material examples. Our study on the colloidal synthesis of InP QDs in the presence of Zn precursors will be discussed, in which size uniformity is markedly enhanced as compared to the case of InP QDs synthesized without Zn precursors. In the presence of zinc carboxylate, intermediate species containing Zn-P bonding appears. The Zn-P intermediate complex with P(SiMe3)3 exhibits lower reactivity than In-P complex. The formation of stable Zn-P intermediate complex results in lower reactivity, hence monodisperse QDs. Insights from the experimental and theoretical studies advance the mechanistic understanding and controlling of nucleation and growth of InP QDs. We investigated diffusion of active species monomers through ligand layers using CdSe nanorods (NRs) as a model system. Colloidal NRs are of special interest for optoelectronic applications because its shape anisotropy leads to unique optical and physical characteristics, expandable with morphological and structural deviation. I present a new answer for detailed growth mechanism of colloidal semiconductor NRs. For this, we developed dual-diameter nanorod (DDNR) structure via colloidal synthesis, where two sections along the long axis in each NR have different diameters at a few nanometer scale. The vivid segmentation is an ideal platform for monitoring the growth process of NRs, presenting important determinants in the reactivity of distinguishable NR facets. By controlling the discovered factors, single-diameter NRs with controllable core position also became available. I will put the findings in perspective by outlining the effect of diffusion of monomers and surface growth reactions.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0010.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.024
GPT teacher head0.262
Teacher spread0.238 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2018
Admission routes1
Has abstractyes

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