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Record W2949339324 · doi:10.1021/acs.macromol.9b00806

Tuning Morphology and Thermal Transport of Asymmetric Smart Polymer Blends by Macromolecular Engineering

2019· article· en· W2949339324 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueMacromolecules · 2019
Typearticle
Languageen
FieldMaterials Science
TopicThermal properties of materials
Canadian institutionsUniversity of British Columbia
FundersCompute Canada
KeywordsPolymer chemistryAcrylic acidHydrogen bondPolymerMonomerContext (archaeology)Chemical engineeringSolubilityvan der Waals forceMaterials sciencePhase (matter)MacromoleculeChemistryMoleculePhysical chemistryOrganic chemistry

Abstract

fetched live from OpenAlex

A grand challenge in designing polymeric materials is to tune their properties by macromolecular engineering. In this context, one of the drawbacks that often limits broader applications of polymers under high temperature conditions is their poor thermal conductivity κ. Using molecular dynamics simulations, we establish a structure–property relationship in hydrogen-bonded polymer blends for possible improvement of κ. For this purpose, we investigate two experimentally relevant hydrogen-bonded systems: one system consists of short poly(N-acryloyl piperidine) (PAP) blended with longer chains of poly(acrylic acid) (PAA), and the second system is a mixture of PAA and short polyacrylamide (PAM) chains. Simulation results show that PAA-PAP blends are at the onset of phase separation over the full range of the PAP monomer mole fraction ϕPAP, which intensifies even more for ϕPAP > 0.3. While PAA and PAP interact with preferential hydrogen bonding, phase separation is triggered by the dominant van der Waals attraction between the hydrophobic side groups of PAP. However, if PAP is replaced with PAM, which has a similar chemical structure as PAP without the hydrophobic side group, PAA-PAM blends show much improved solubility. Better solubility is due to the preferential hydrogen bonding between PAA and PAM. As a result, PAM oligomers act as cross-linking bridges between PAA chains resulting in a three-dimensional highly cross-linked network. While κ for PAA-PAP blends remain almost invariant with ϕPAP, PAA-PAM systems show improved κ with increasing PAM concentration and also with respect to PAA-PAP blends. Consistent with the theoretical prediction for the thermal transport of amorphous polymers, we show that κ is proportional to the materials’ stiffness, that is, the bulk modulus K and sound velocity v of PAA-PAM blends. However, no functional dependence between κ and K (or v) is observed for the immiscible PAA-PAP blends.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.005
GPT teacher head0.188
Teacher spread0.183 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it