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Record W2950353302 · doi:10.1021/cm000743j

The Effect of Interlayer Cations on the Magnetic Properties of the Mixed-Metal Pnictide Oxides:  A<sub>2</sub>MnZn<sub>2</sub>As<sub>2</sub>O<sub>2</sub> (A = Sr, Ba)

2001· article· en· W2950353302 on OpenAlexaff
Tadashi C. Ozawa, Susan M. Kauzlarich, Mario Bieringer, C. R. Wiebe, John E. Greedan, J. S. Gardner

Bibliographic record

VenueChemistry of Materials · 2001
Typearticle
Languageen
FieldMaterials Science
TopicMagnetic and transport properties of perovskites and related materials
Canadian institutionsMcMaster UniversityAtomic Energy (Canada)
Fundersnot available
KeywordsMaterials scienceRietveld refinementNeutron diffractionMagnetizationStoichiometryCrystallographyPnictogenPowder diffractionMagnetic susceptibilityCrystal structureAtmospheric temperature rangeDiffractionX-ray crystallographyPhase (matter)Analytical Chemistry (journal)Condensed matter physicsChemistrySuperconductivityPhysical chemistryOpticsMagnetic field

Abstract

fetched live from OpenAlex

The new pnictide oxide Sr 2 MnZn 2 As 2 O 2 is reported. The crystal structure of this compound consists of a 1:1 intergrowth of square-planar MnO 2 2 - layers and ThCr 2 Si 2 -type Zn 2 As 2 2 - layers interspersed by Sr cations. This compound has been prepared by sintering the stoichiometric ratio of SrO, Mn, Zn, and As in a fused-silica ampule under 0.2 atm of Ar at 1000 °C for 1 week. The sample quality has been examined by Rietveld refinement of the powder X-ray diffraction data, and the transition metal site (2a and 4d) selectivity has been analyzed by Rietveld refinement of powder neutron diffraction data. Furthermore, effects of this structural order on the magnetic susceptibility and interaction between the magnetic layers have been analyzed by temperature-dependent magnetization measurements. The magnetic structures of both phases, A 2 MnZn 2 As 2 O 2 (A = Sr, Ba), have been investigated by temperature-dependent powder neutron diffraction. The Ba analogue exhibits two-dimensional short-range order below about 40 K, whereas for the Sr analogue, no evidence for either long- or short-range order was found over the 2θ range investigated down to 4 K. The results of these characterizations are compared with those of the previously studied phase, Sr 2 Mn 3 As 2 O 2 .

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.189
Teacher spread0.182 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations25
Published2001
Admission routes1
Has abstractyes

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