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Record W2950477686 · doi:10.1139/v99-241

Theoretical studies of azulene and its derivatives

2000· article· en· W2950477686 on OpenAlexvenueno aff
Wen‐Jwu Wang, Yun‐Shan Lin, Jian‐Chuang Chang, Peiyu Wang

Bibliographic record

VenueCanadian Journal of Chemistry · 2000
Typearticle
Languageen
FieldMaterials Science
TopicPhotochromic and Fluorescence Chemistry
Canadian institutionsnot available
FundersNational Science Council
KeywordsAzuleneChemistryAb initioBasis setExcited stateComputational chemistryAb initio quantum chemistry methodsGround stateDensity functional theoryMoleculePhotochemistryOrganic chemistryAtomic physics

Abstract

fetched live from OpenAlex

The results of ab initio calculations with the 6-31G basis sets on azulene and its derivatives (including azulenequinones and diazoazulenequinones) are presented in accordance with considerations of their structures and bonding. Azulene is a non-alternant compound with ten π electrons and has either a C s or C 2v symmetry depending on the different carbon bonding. The semiempirical and HF ab initio calculations converge to a C s symmetry and the DFT and MP2 calculations converge to a C 2v symmetry as a ground state structure of azulene. The CIS calculations describe the excited state of azulene and the first excitation energy (S 0 - S 1 ) is 533 nm (CIS/6-31+G * ), which could illustrate the azure color of azulene. According to the geometry analysis, there are 16 geometrical isomers in azulenequinone conjugated diketones of azulene. Ab initio calculation with the 6-31G basis set generates 1,5- and 1,7-azulenequinone being the most stable isomers of azulenequinone. Theoretically, the relative stability of the bromination product of azulenequinones indicates that 7-bromo-1,5-azulenequinone and 3-bromo-1,7- azulenequinone (for monobromoazulenequinones) and 3,7-dibromo-1,5- azulenequinone and 3,5-dibromo-1,7-azulenequinone (for dibromoazulenequinones) are more stable isomers. The product of diazotization of amino- bromoazulenes is diazoazulenequinone in which a diazo group replaces a ketone group. Isomeric 1,8- and 1,2-diazoazulenequinones are the most stable isomers of diazoazulenequinone according to the theoretical consideration. Due to the resonance and relative stability, diazoazulenequinone may easily extrude nitrogen and form the corresponding triplet ketocarbene intermediate and electronic isomers that undergo photoreaction with THF leading to a polyether bridged azulene (crown type ether). The cyclic reactions in diazoazulenequinone are also studied.Key words: azulene, azulenequinone, diazoazulenequinone, ab initio.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.007
Threshold uncertainty score0.995

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0060.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.015
GPT teacher head0.246
Teacher spread0.231 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations9
Published2000
Admission routes1
Has abstractyes

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