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Record W2951533295 · doi:10.1021/acs.macromol.9b00794

Thermoresponsive Behavior of Poly(acrylic acid-<i>co</i>-acrylonitrile) with a UCST

2019· article· en· W2951533295 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueMacromolecules · 2019
Typearticle
Languageen
FieldChemistry
TopicAdvanced Polymer Synthesis and Characterization
Canadian institutionsUniversité de Montréal
FundersChina Scholarship CouncilNatural Science Foundation of Zhejiang ProvinceNatural Sciences and Engineering Research Council of CanadaNational Natural Science Foundation of China
KeywordsUpper critical solution temperatureCopolymerAcrylonitrileMicellePolymer chemistryAcrylic acidPolymerHydrogen bondAmphiphileMaterials scienceCloud pointChemical engineeringMiscibilityHydrophobic effectAqueous solutionChemistryLower critical solution temperatureOrganic chemistryMoleculeComposite material

Abstract

fetched live from OpenAlex

Poly(acrylic acid) is water soluble but can be converted into a thermoresponsive polymer possessing an upper critical solution temperature (UCST) by copolymerizing with acrylonitrile. The copolymers showed a UCST in water under ambient conditions, driven by the combined effect of hydrogen bonding between the carboxylic acid groups and hydrophobic interaction among the acrylonitrile moieties. The cloud point of the copolymers can be tuned by changing the copolymer composition, concentration, pH, and ionic strength of the solution. The dynamic light scattering results indicate that the amphiphilic copolymer chains are solubilized in the form of micelles through interchain hydrophobic interaction and the micelles may also form small aggregates through hydrogen bonding at temperatures below the UCST. This work demonstrates a new strategy for the design of thermoresponsive polymers from comonomers that are not known to produce thermoresponsive polymers but can be made into such polymers through the synergetic effect of different interactions that contribute to the enthalpic and entropic changes of mixing in the aqueous systems.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.017
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.230
Teacher spread0.223 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it