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Record W2963841441 · doi:10.1002/prep.201900093

Preparation of Cyclotrimethylenetrinitramine‐Copper Oxide Core‐Shell Particles and Their Thermal Decomposition Kinetics

2019· article· en· W2963841441 on OpenAlexaff
Xiang Zhou, Ying Zhu, Zhipeng Cheng, Xiang Ke, Kaiwen Shi, Kaili Zhang

Bibliographic record

VenuePropellants Explosives Pyrotechnics · 2019
Typearticle
Languageen
FieldMaterials Science
TopicThermal and Kinetic Analysis
Canadian institutionsMinistry of Education and Child Care
FundersFundamental Research Funds for the Central UniversitiesNanjing University of Science and TechnologyNatural Science Foundation of Jiangsu ProvinceNational Natural Science Foundation of China
KeywordsThermal decompositionMaterials scienceDecompositionThermogravimetric analysisCopper oxideCopperKineticsActivation energyOxideThermal stabilityChemical engineeringGravimetric analysisEnergetic materialAnalytical Chemistry (journal)Physical chemistryExplosive materialChemistryMetallurgyOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract The effect of interfacial contact conditions between cyclotrimethylenetrinitramine (RDX) and copper oxide (CuO) on the thermal decomposition kinetics of RDX was investigated in this study. CuO was deposited onto the surface of superfine RDX particles to form RDX@CuO core‐shell structure through RF magnetron sputtering technology. The thermal decomposition characteristics of RDX, RDX@CuO and RDX‐CuO ultrasonic mixture were studied through thermo‐gravimetric method. Kissinger and Kissinger‐Akahira‐Sunose methods were used to obtain kinetic parameters of thermal decomposition processes. It was found that the temperature corresponding to maximum weight loss rate decreased in the order of RDX>RDX‐CuO>RDX@CuO. However, the apparent activation energy of RDX decomposition did not show apparent difference for the two kinds of CuO‐containing samples. The results indicate that the interfacial contact conditions between RDX and CuO have an effect on the thermal stability of RDX but do not alter the thermal decomposition paths of RDX.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.002

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.019
GPT teacher head0.271
Teacher spread0.252 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations16
Published2019
Admission routes1
Has abstractyes

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