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Record W2963841441 · doi:10.1002/prep.201900093

Preparation of Cyclotrimethylenetrinitramine‐Copper Oxide Core‐Shell Particles and Their Thermal Decomposition Kinetics

2019· article· en· W2963841441 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenuePropellants Explosives Pyrotechnics · 2019
Typearticle
Languageen
FieldMaterials Science
TopicThermal and Kinetic Analysis
Canadian institutionsMinistry of Education and Child Care
FundersFundamental Research Funds for the Central UniversitiesNanjing University of Science and TechnologyNatural Science Foundation of Jiangsu ProvinceNational Natural Science Foundation of China
KeywordsThermal decompositionMaterials scienceDecompositionThermogravimetric analysisCopper oxideCopperKineticsActivation energyOxideThermal stabilityChemical engineeringGravimetric analysisEnergetic materialAnalytical Chemistry (journal)Physical chemistryExplosive materialChemistryMetallurgyOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract The effect of interfacial contact conditions between cyclotrimethylenetrinitramine (RDX) and copper oxide (CuO) on the thermal decomposition kinetics of RDX was investigated in this study. CuO was deposited onto the surface of superfine RDX particles to form RDX@CuO core‐shell structure through RF magnetron sputtering technology. The thermal decomposition characteristics of RDX, RDX@CuO and RDX‐CuO ultrasonic mixture were studied through thermo‐gravimetric method. Kissinger and Kissinger‐Akahira‐Sunose methods were used to obtain kinetic parameters of thermal decomposition processes. It was found that the temperature corresponding to maximum weight loss rate decreased in the order of RDX>RDX‐CuO>RDX@CuO. However, the apparent activation energy of RDX decomposition did not show apparent difference for the two kinds of CuO‐containing samples. The results indicate that the interfacial contact conditions between RDX and CuO have an effect on the thermal stability of RDX but do not alter the thermal decomposition paths of RDX.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.589

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.019
GPT teacher head0.271
Teacher spread0.252 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it