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Record W2971621573 · doi:10.3749/canmin.1900025

Nickeltyrrellite, CuNi2Se4, a new member of the spinel supergroup from El DragÓn, Bolivia

2019· article· en· W2971621573 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

venuePublished in a venue whose home country is Canada.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueThe Canadian Mineralogist · 2019
Typearticle
Languageen
FieldMaterials Science
TopicCrystal Structures and Properties
Canadian institutionsnot available
FundersNatural Environment Research CouncilSight Research UK
KeywordsPleochroismCrystallographyMaterials scienceMineralogyAnalytical Chemistry (journal)Electron backscatter diffractionChemistryCrystal structure

Abstract

fetched live from OpenAlex

Abstract Nickeltyrrellite, ideally CuNi2Se4, is a new selenide species from the El Dragón mine, Department of Potosí, Bolivia. It most frequently occurs as anhedral to subhedral grains (up to 20 μm in size) in association with cerromojonite, klockmannite, clausthalite, and penroseite, forming fracture fillings in pre-existing krut'aite−penroseite solid solutions. Nickeltyrrellite is non-fluorescent, black, and opaque with a metallic luster and black streak. It is brittle, with an irregular fracture and no obvious cleavage and parting. In plane-polarized incident light, nickeltyrrellite is cream to pale pinkish, displaying no internal reflections. Between crossed polarizers, it is isotropic. The reflectance values in air for the COM standard wavelengths are 45.9 (470 nm), 47.6 (546 nm), 48.1 (589 nm), and 49.8 (650 nm). Electron-microprobe spot analyses (n = 28) of the grain populations used for the EBSD study yielded a mean composition of Cu 13.01, Fe 0.27, Co 6.66, Ni 16.98, S 1.04, Se 61.91, total 99.87 wt.%. The empirical formula, normalized to 7 apfu, is Cu1.00(Ni1.42Co0.56Fe0.02)Σ2.00(Se3.84S0.16)Σ4.00. The ideal formula is CuNi2Se4, which requires (in wt.%) Cu 12.79, Ni 23.63, Se 63.58, total 100. EBSD patterns reveal nickeltyrrellite as cubic, space group , with a = 9.99 Å, V = 997.0 Å3, Z = 8. The calculated density is 7.36 g cm−3. It formed in response to alteration of quijarroite + hansblockite + watkinsonite + clausthalite + penroseite aggregates by oxidizing, low-T, Cu-Ni-Co-Pb-bearing fluids at a fSe2/fS2 ratio greater than unity. Nickeltyrrellite is a new selenide belonging to the tyrrellite subgroup of the spinel supergroup. The new species has been approved by the IMA-CNMNC (2018-110) and is named for constituting the Ni-analogue of tyrrellite.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.840
Threshold uncertainty score0.996

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0050.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.213
Teacher spread0.198 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it