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Record W2975190380 · doi:10.5006/3294

A Mechanistic Study of Carbon Steel Cracking in 360°C Air and Hydrogen Environments

2019· article· en· W2975190380 on OpenAlexaff
S.Y. Persaud, Koji Arioka, K. Farquharson, C.E. Dixon, C. D. Judge

Bibliographic record

VenueCORROSION · 2019
Typearticle
Languageen
FieldMaterials Science
TopicHydrogen embrittlement and corrosion behaviors in metals
Canadian institutionsCanadian Nuclear LaboratoriesQueen's University
Fundersnot available
KeywordsMaterials scienceCreepCementiteCrackingMetallurgyCarbon fibersHydrogenAmorphous carbonFerrite (magnet)Intergranular corrosionHydrogen embrittlementStress corrosion crackingComposite materialComposite numberAmorphous solidCorrosionAusteniteMicrostructureChemistry

Abstract

fetched live from OpenAlex

Thirty percent cold-worked (CW) carbon steel tensile specimens were exposed to 360°C air and hydrogen environments (2 MPa H2 and 20 MPa H2) under an applied load to produce intergranular creep cracking. In this study, cutting-edge microscopy techniques were applied to characterize cracking on multiple length scales and in three dimensions. The objective was to develop a better mechanistic understanding of creep cracking in carbon steel, and the known deleterious effect of hydrogen (attack) at the micro-to-nanoscale. Amorphous carbon along the fracture path was observed in all experiments, with evidence for nanoscale cavities/methane bubbles in hydrogen exposures, particularly at cementite-ferrite boundaries. Results suggested that creep or residual stress led to breakdown of cementite to amorphous carbon, cavitation, and/or formation of methane (depending on H2 content); it is suggested that the combination of deleterious mechanisms leads to initiation and/or acceleration of creep cracking in CW carbon steel. Comparisons are made between the morphology of creep cracking in these laboratory experiments and recent results from characterization of creep cracking in ex-service carbon steel piping from a CANDU nuclear power plant. Although more subtle, similar morphology and chemistry at crack tips in laboratory and ex-service CW carbon steel suggests that the mechanism(s) of creep cracking is similar.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.142
Threshold uncertainty score0.550

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.246
Teacher spread0.232 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations1
Published2019
Admission routes1
Has abstractyes

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