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Record W2977523176 · doi:10.1002/advs.201902170

Heterostructure Engineering of a Reverse Water Gas Shift Photocatalyst

2019· article· en· W2977523176 on OpenAlex
Hong Wang, Jia Jia, Lu Wang, Keith T. Butler, Rui Song, Gilberto Casillas, Le He, Nazir P. Kherani, Doug D. Perovic, Liqiang Jing, Aron Walsh, Roland Dittmeyer, Geoffrey A. Ozin

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueAdvanced Science · 2019
Typearticle
Languageen
FieldEnergy
TopicAdvanced Photocatalysis Techniques
Canadian institutionsUniversity of Toronto
FundersOntario Ministry of Research and InnovationNatural Sciences and Engineering Research Council of CanadaMinistero dello Sviluppo EconomicoNankai UniversityUniversity of TorontoNational Natural Science Foundation of ChinaAlexander von Humboldt-StiftungLions Clubs International FoundationNational Science Foundation
KeywordsNanorodPhotocatalysisHeterojunctionMaterials scienceCatalysisOxideNiobium pentoxideNiobium oxideNanocrystalChemical engineeringIndiumNanotechnologyChemistryNiobiumOptoelectronicsOrganic chemistryMetallurgy

Abstract

fetched live from OpenAlex

Abstract To achieve substantial reductions in CO 2 emissions, catalysts for the photoreduction of CO 2 into value‐added chemicals and fuels will most likely be at the heart of key renewable‐energy technologies. Despite tremendous efforts, developing highly active and selective CO 2 reduction photocatalysts remains a great challenge. Herein, a metal oxide heterostructure engineering strategy that enables the gas‐phase, photocatalytic, heterogeneous hydrogenation of CO 2 to CO with high performance metrics (i.e., the conversion rate of CO 2 to CO reached as high as 1400 µmol g cat −1 h −1 ) is reported. The catalyst is comprised of indium oxide nanocrystals, In 2 O 3− x (OH) y , nucleated and grown on the surface of niobium pentoxide (Nb 2 O 5 ) nanorods. The heterostructure between In 2 O 3− x (OH) y nanocrystals and the Nb 2 O 5 nanorod support increases the concentration of oxygen vacancies and prolongs excited state (electron and hole) lifetimes. Together, these effects result in a dramatically improved photocatalytic performance compared to the isolated In 2 O 3− x (OH) y material. The defect optimized heterostructure exhibits a 44‐fold higher conversion rate than pristine In 2 O 3− x (OH) y . It also exhibits selective conversion of CO 2 to CO as well as long‐term operational stability.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.019
Threshold uncertainty score0.666

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.004
GPT teacher head0.229
Teacher spread0.225 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it