Preparation of spherical aminopropyl-functionalized MCM-41 and its application in removal of Pb(II) ion from aqueous solution
Why this work is in the frame
A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.
Bibliographic record
Abstract
Abstract Mesoporous silica microspheres were prepared by the polymerization-induced colloid aggregation (PICA) and pseudomorphic synthesis methods. The prepared microspheres have high specific surface area and MCM-41 type structure. In the PICA process, acidic silica sol was utilized as silica source and the effect of molar ration (formaldehyde/urea) was investigated. Moreover, the influences of reaction time and temperature were also studied. The specific surface area of porous and mesoporous silica microspheres were 186.4 m2/g and 900.4 m2/g, respectively. The materials were characterized by SAXS, FTIR, SEM, TEM and nitrogen sorption measurements. The prepared silica microspheres were functionalized by (3-Aminopropyl)triethoxysilane and then used to remove the lead from aqueous solution. The result indicates that the grafted silica microspheres have rapid adsorption capacity and good reproducibility. The adsorption data was fitted well with the Langmuir isotherm model, and the maximum adsorption capacities for MCM-41 silica microspheres were 102.7 mg/g.
Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.
Full frame distilled prediction
Teacher imitationNot calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.
Codex and Gemma teacher scores by category
| Category | Codex | Gemma |
|---|---|---|
| Metaresearch | 0.001 | 0.000 |
| Meta-epidemiology (narrow) | 0.000 | 0.000 |
| Meta-epidemiology (broad) | 0.001 | 0.000 |
| Bibliometrics | 0.000 | 0.000 |
| Science and technology studies | 0.000 | 0.000 |
| Scholarly communication | 0.000 | 0.000 |
| Open science | 0.000 | 0.000 |
| Research integrity | 0.000 | 0.000 |
| Insufficient payload (model declined to judge) | 0.000 | 0.000 |
Machine scores (provisional)
The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.
Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.
score_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it