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Record W2999706242 · doi:10.3749/canmin.1900051

Okieite, Mg3[V10O28]·28H2O, a new decavanadate mineral from the Burro mine, Slick Rock mining district, San Miguel County, Colorado, USA

2020· article· en· W2999706242 on OpenAlex
Anthony R. Kampf, P. M. Adams, Barbara P. Nash, Joe Marty, John M. Hughes

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

venuePublished in a venue whose home country is Canada.
no affNo Canadian affiliation: this work is invisible to an affiliation-only frame.
No Canadian affiliation. An affiliation-only frame, the usual design, would never have seen this work. It is one of the works that make the case for inverting the frame.

Bibliographic record

VenueThe Canadian Mineralogist · 2020
Typearticle
Languageen
FieldMaterials Science
TopicPolyoxometalates: Synthesis and Applications
Canadian institutionsnot available
Fundersnot available
KeywordsPleochroismTriclinic crystal systemCrystallographyMineralMohs scale of mineral hardnessMineralogyChemistryElectron probe microanalysisCleavage (geology)Crystal structureMaterials scienceElectron microprobeFracture (geology)Composite material

Abstract

fetched live from OpenAlex

ABSTRACT Okieite, Mg3[V10O28]·28H2O, is a new decavanadate mineral from the Burro mine, Slick Rock district, San Miguel County, Colorado, USA (type locality); the mineral is also found at the Hummer mine, Paradox Valley, Montrose County, also in Colorado. The mineral is rare; it occurs with dickthomssenite on montroseite- and corvusite-bearing sandstone. Crystals of okieite from the Burro mine are equant to prismatic, commonly appearing like curving columns (up to about 3 mm in length) and often exhibiting rounded faces. The streak of okieite is light orange yellow, and the luster is vitreous. The Mohs hardness is ca. 1½, the tenacity is brittle, the fracture is curved or conchoidal, there is no cleavage, and the measured density is 2.20(2) g/cm3. Okieite is biaxial (–), with α = 1.720(3), β = 1.745(3), γ = 1.765(3) (white light); 2V = 84(2)° with strong r < v dispersion. The optical orientation is X ^ a = 37°, Y ^ c = 28°, Z ^ b = 31°. No pleochroism is observed in okieite. The empirical formula from electron-probe microanalysis (calculated on the basis of V = 10 and O = 56 apfu as indicated by the structure) is Mg2.86[H0.28V5+10O28]·28H2O. Okieite is triclinic, , with a 10.55660(19), b 10.7566(2), c 21.3555(15)Å, α 90.015(6), β 97.795(7), γ 104.337(7)°, and V 2326.30(19)Å3, as determined by single-crystal X-ray diffractometry. The strongest four diffraction lines in the powder diffractograms are [d in Å(I)(hkl)]: 9.71(100); 8.32(19); 11.04(17)(002); and 6.42(12)(110, . The atomic arrangement of okieite [R1 = 0.0352 for 11,327 I > 2σI reflections] consists of a {V10O28}6– (decavanadate) structural unit and a {[Mg(H2O)6]3·10H2O}6+ interstitial complex. Only hydrogen bonding links the structural unit with the components of the interstitial complex. Okieite is isostructural with synthetic Mg3[V10O28]·28H2O. The name okieite is for Craig (“Okie”) Howell of Naturita, Colorado.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Not applicable · Consensus signal: Not applicable
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.172
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0010.000
Scholarly communication0.0010.000
Open science0.0020.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.040
GPT teacher head0.240
Teacher spread0.200 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it