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Record W3038301407 · doi:10.1021/acscentsci.0c00604

Atomically Dispersed Iridium on Indium Tin Oxide Efficiently Catalyzes Water Oxidation

2020· article· en· W3038301407 on OpenAlexfundno aff
Dmitry Lebedev, Roman Ezhov, Javier Heras‐Domingo, Aleix Comas‐Vives, Nicolas Kaeffer, Marc‐Georg Willinger, Xavier Solans‐Monfort, Xing Huang, Yulia Pushkar, Christophe Copéret

Bibliographic record

VenueACS Central Science · 2020
Typearticle
Languageen
FieldEnergy
TopicElectrocatalysts for Energy Conversion
Canadian institutionsnot available
FundersCanadian Light SourceBasic Energy SciencesDivision of ChemistryOffice of ScienceUniversity of WashingtonNational Science FoundationInnosuisse - Schweizerische Agentur für InnovationsförderungMinisterio de Economía y CompetitividadGeneralitat de CatalunyaEuropean Social FundArgonne National LaboratoryU.S. Department of Energy
KeywordsIridiumCatalysisOxygen evolutionIndiumTinElectrochemistryIndium tin oxideOxideTransition metalMaterials scienceInorganic chemistryRedoxOxidation stateMetalNanotechnologyChemical engineeringChemistryElectrodePhysical chemistryThin filmOrganic chemistryMetallurgy

Abstract

fetched live from OpenAlex

High Resolution Image Download MS PowerPoint Slide Heterogeneous catalysts in the form of atomically dispersed metals on a support provide the most efficient utilization of the active component, which is especially important for scarce and expensive late transition metals. These catalysts also enable unique opportunities to understand reaction pathways through detailed spectroscopic and computational studies. Here, we demonstrate that atomically dispersed iridium sites on indium tin oxide prepared via surface organometallic chemistry display exemplary catalytic activity in one of the most challenging electrochemical processes, the oxygen evolution reaction (OER). In situ X-ray absorption studies revealed the formation of Ir V ═O intermediate under OER conditions with an Ir–O distance of 1.83 Å. Modeling of the reaction mechanism indicates that Ir V ═O is likely a catalyst resting state, which is subsequently oxidized to Ir VI enabling fast water nucleophilic attack and oxygen evolution. We anticipate that the applied strategy can be instrumental in preparing and studying a broad range of atomically dispersed transition metal catalysts on conductive oxides for (photo)electrochemical applications.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.210
Teacher spread0.201 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations77
Published2020
Admission routes1
Has abstractyes

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