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Record W3040223952 · doi:10.1107/s2053273319090624

Efficient recognition of steroids by planar aromatic molecules: a novel biomolecular recognition motif and its potential applications

2019· article· en· W3040223952 on OpenAlexaff
Filip Topić, Tomislav Friščić

Bibliographic record

VenueActa Crystallographica Section A Foundations and Advances · 2019
Typearticle
Languageen
FieldChemistry
TopicMolecular Sensors and Ion Detection
Canadian institutionsMcGill University
Fundersnot available
KeywordsMotif (music)Molecular recognitionPlanarMoleculeChemistryNanotechnologyComputational biologyMaterials scienceComputer scienceBiologyPhysicsOrganic chemistryComputer graphics (images)

Abstract

fetched live from OpenAlex

Traditionally, functional groups attached to the backbone of steroid molecules were seen as the key factors in their molecular recognition and, consequently, their physiological function.However, a systematic study of the cocrystals of steroids with electron-rich, planar aromatic molecules (arenes) by our group has recently revealed the ••• interaction: a previously undescribed interaction mode of steroids involving the -face of a steroid and theelectron system of aromatic molecules.Progesterone was found to reliably engage in ••• interaction with various arenes, whereas other steroids studied so far suggest a strong dependence of this interaction on the fine structural details of the steroid backbone.This mimics the steroid behavior in the biological systems, where small structural differences give rise to significantly different biological functions.We set out to pursue the cocrystallization of progesterone with a variety of polyaromatic hydrocarbons and heterocycles using the mechanochemical solid-state screening methods developed in our group.Furthermore, we sought to expand the set of steroid cocrystal formers towards biologically and pharmaceutically relevant adrenosterone (a weak androgen), cholest-4-en-3-one (metabolite of cholesterol), exemestane (anticancer drug) and levonorgestrel (used in birth control), all of which exhibit a degree of structural similarity with progesterone.Finally, we investigated the possibility of combining the ••• interaction with known interactions such as hydrogen and halogen bonding to engineer increasingly complex molecular solids.This presentation will outline our initial findings, which confirm the reliability of the ••• interactions and establish its applicability to steroid molecules beyond progesterone.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.005

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.219
Teacher spread0.211 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2019
Admission routes1
Has abstractyes

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