MétaCan
Menu
Back to cohort

LC-MS characterization of antibody-based therapeutics

2020· book-chapter· en· W3080304030 on OpenAlexaff
Anna Robotham, John F. Kelly

Bibliographic record

VenueElsevier eBooks · 2020
Typebook-chapter
Languageen
FieldMedicine
TopicMonoclonal and Polyclonal Antibodies Research
Canadian institutionsNational Research Council Canada
Fundersnot available
KeywordsAntibodyComputational biologyPaceCharacterization (materials science)ChemistryComputer scienceNanotechnologyMedicineBiologyMaterials scienceImmunologyGeography

Abstract

fetched live from OpenAlex

Antibody-based therapeutics constitute a major growth area in medicine today. However, antibodies as drugs present significant analytical challenges as they are large, complex and heterogenous molecules produced in living cells. The key attributes that affect safety, stability and efficacy must be identified and controlled to ensure regulatory compliance. Liquid Chromatography-Mass Spectrometry (LC-MS) is a powerful analytical technology that is well suited to the task of analyzing antibody-based therapeutics. LC-MS is used to characterize antibody features ranging from the relatively simple (e.g. intact molecular weight determination and post-translational modification analysis) to the complex (e.g., higher order structure analysis and epitope identification). Few other analytical technologies are as versatile as LC-MS for monitoring a wide range of attributes or as capable of keeping pace with the innovation happening today in biotherapeutic design. In this chapter we will provide an overview of the LC-MS methods currently used for the characterization of antibody-based therapeutics, with an emphasis on the analysis of post-translational modifications. We will also highlight some recent innovations, new technologies and trends that are likely to significantly impact the manner in which antibody-based therapeutics are analyzed in the future.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Methods · Consensus signal: none
Teacher disagreement score0.007
Threshold uncertainty score0.023

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.001
Science and technology studies0.0000.000
Scholarly communication0.0010.000
Open science0.0000.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0070.008

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.039
GPT teacher head0.310
Teacher spread0.271 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreMethods

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations13
Published2020
Admission routes1
Has abstractyes

Explore more

Same venueElsevier eBooksSame topicMonoclonal and Polyclonal Antibodies ResearchFrench-language works237,207