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Record W3083630282 · doi:10.1080/01418610108214433

Deformation of copper single crystals to large strains at 4.2 K

2001· article· en· W3083630282 on OpenAlexaff
M. Niewczas, Z. S. Basinski, J.D. Embury

Bibliographic record

VenuePhilosophical magazine. A/Philosophical magazine. A. Physics of condensed matter. Structure, defects and mechanical properties · 2001
Typearticle
Languageen
FieldMaterials Science
TopicMicrostructure and mechanical properties
Canadian institutionsMcMaster University
Fundersnot available
KeywordsSubstructureAnnealing (glass)Materials scienceDislocationElectrical resistivity and conductivityTransmission electron microscopyDipoleVacancy defectCrystallographyCopperCondensed matter physicsComposite materialMetallurgyNanotechnologyChemistry

Abstract

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Transmission electron microscopy (TEM) observations of the dislocation substructure developed in high-purity single crystals of Cu deformed at 4.2 K have been carried out in order to relate the detailed defect structures to the mechanical and electrical properties discussed in part I. The results based on weak-beam TEM show that the dislocation substructure contains a very high density of narrow dislocation dipoles of vacancy character. These dipoles become progressively refined in scale as deformation continues. In-situ annealing experiments carried out in the transmission electron microscope allow the stability of these structures against annealing at room temperature and elevated temperatures to be studied. The observations suggest that fine dislocation dipoles can be annealed by processes such as pipe diffusion and that these defects represent the recoverable component of electrical resistivity. For comparison some studies were undertaken in Cu-5 at.% Ni single crystals which indicate that the recoverable component of resistivity in this alloy is smaller owing to the influence of the Ni on the pipe diffusion process. In addition, TEM studies indicate the complexity of processes occurring at the twin-parent interfaces produced in Cu deformed at 4.2 K. These interfaces have an important role in debris storage and in processes that can occur after large plastic strains at 4.2 K.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score0.012

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0010.000
Scholarly communication0.0010.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.031
GPT teacher head0.242
Teacher spread0.211 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations34
Published2001
Admission routes1
Has abstractyes

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Same venuePhilosophical magazine. A/Philosophical magazine. A. Physics of condensed matter. Structure, defects and mechanical propertiesSame topicMicrostructure and mechanical propertiesFrench-language works237,207