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Record W3084403848 · doi:10.1021/acs.analchem.0c01287

Experimental Evidence of Enhanced Adsorption Dynamics at Liquid–Liquid Interfaces under an Electric Field

2020· article· en· W3084403848 on OpenAlexaff
Sameer Mhatre, Sébastien Simon, Johan Sjöblom

Bibliographic record

VenueAnalytical Chemistry · 2020
Typearticle
Languageen
FieldChemistry
TopicElectrochemical Analysis and Applications
Canadian institutionsUniversity of Calgary
Fundersnot available
KeywordsChemistryAdsorptionElectric fieldDynamics (music)Chemical physicsLiquid liquidField (mathematics)NanotechnologyChromatographyPhysical chemistry

Abstract

fetched live from OpenAlex

In this work, we investigate the adsorption of surface-active compounds at the water–oil interface subjected to an electric field. A fluid system comprising a pendent water drop surrounded by an asphaltene-rich organic phase is exposed to a DC uniform electric field. Two subfractions of asphaltenes having contrasting affinities to the water–oil interface are used as surface-active compounds. The microscopic changes in the drop shape, as a result of asphaltene adsorption, are captured and the drop profiles are analyzed using our in-house code for axisymmetric drop shape analysis (ADSA) under an electric field. The estimates of dynamic interfacial tension under different strengths of the field (E0) and concentrations of the asphaltene subfractions (C) are used to calculate adsorption dynamics and surface excess. The experimental observations and careful analyses of the data suggest that the externally applied electric field significantly stimulates the mass-transfer rate at the liquid–liquid interface. The enhancement in mass transport at the water–oil interface can be attributed to the axisymmetric electrohydrodynamic fluid flows generated on either side of the interface. The boost in mass transport is evident from the growing decay in equilibrium interfacial tension (γeq) and increased surface excess (Γeq) upon increasing strength of the applied electric field. The mass-transfer intensification does not increase monotonously with the electric field strength above an optimum E0, which is in agreement with the previous theoretical studies in the literature. However, these first explicit experimental measurements of adsorption at an interface under an electric field suggest that the optimum E0 is determined by characteristics of the surface-active molecules.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.019
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.022
GPT teacher head0.296
Teacher spread0.275 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations12
Published2020
Admission routes1
Has abstractyes

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