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Time-resolved imaging of carrier transport in halide perovskite thin films and evidence for nondiffusive transport

2019· article· en· W3099577632 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenuePhysical Review Materials · 2019
Typearticle
Languageen
FieldEngineering
TopicPerovskite Materials and Applications
Canadian institutionsPolytechnique Montréal
FundersOffice of Naval ResearchNatural Sciences and Engineering Research Council of Canada
KeywordsMaterials scienceHalidePerovskite (structure)Thin filmOptoelectronicsChemical engineeringNanotechnologyInorganic chemistry

Abstract

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Owing to their exceptional semiconducting properties, hybrid inorganic-organic perovskites show great promise as photovoltaic absorbers. In these materials, long-range diffusion of charge carriers allows for most of the photogenerated carriers to contribute to the photovoltaic efficiency. Here, time-resolved photoluminescence (PL) microscopy is used to directly probe ambipolar carrier diffusion and recombination kinetics in hybrid perovskites. This technique is applied to thin films of methylammonium lead tri-iodide $(\mathrm{MAPb}{\mathrm{I}}_{3})$ obtained with two different fabrication routes, methylammonium lead tribromide $(\mathrm{MAPbB}{\mathrm{r}}_{3})$, and an alloy of formamidinium lead tri-iodide and methylammonium lead bromide $\mathrm{F}{\mathrm{A}}_{0.85}\mathrm{M}{\mathrm{A}}_{0.15}\mathrm{Pb}{({\mathrm{I}}_{0.85}\mathrm{B}{\mathrm{r}}_{0.15})}_{3}$. Average diffusion coefficients in the films leading to the highest device efficiencies and longest lifetimes, i.e., in $\mathrm{F}{\mathrm{A}}_{0.85}\mathrm{M}{\mathrm{A}}_{0.15}\mathrm{Pb}{({\mathrm{I}}_{0.85}\mathrm{B}{\mathrm{r}}_{0.15})}_{3}$ and acetonitrile-processed $\mathrm{MAPb}{\mathrm{I}}_{3}$, are found to be several orders of magnitude lower than in the other films. Further examination of the time dependence shows strong evidence for nondiffusive transport. In particular, acetonitrile-processed $\mathrm{MAPb}{\mathrm{I}}_{3}$ shows distinct diffusion regimes on short and long timescales with an effective diffusion constant varying over 2 orders of magnitude. Our results also highlight the fact that increases in carrier lifetime in this class of materials are not necessarily concomitant with increased diffusion lengths and that the PL quantum efficiency under solar cell operating conditions is a greater indication of material, and ultimately device, quality.

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Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.069
Threshold uncertainty score0.713

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.016
GPT teacher head0.285
Teacher spread0.269 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it