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Record W3102896769 · doi:10.22215/etd/2020-14206

Development and characterization of aptamer-conjugated imaging tools for diagnostic applications

2020· dissertation· en· W3102896769 on OpenAlexaff
Anna Koudrina

Bibliographic record

Venuenot available
Typedissertation
Languageen
FieldMaterials Science
TopicNanoparticle-Based Drug Delivery
Canadian institutionsCarleton University
Fundersnot available
KeywordsFibrinFibrinogenIsothermal titration calorimetryChemistryMagnetic resonance imagingDOTABiomedical engineeringMedicineBiochemistryRadiologyImmunologyChelationOrganic chemistry

Abstract

fetched live from OpenAlex

Magnetic resonance imaging (MRI) and computed tomography (CT) are imaging modalities commonly used to assess blood flow; however, neither can label a blood clot that may either disrupt flow, causing an ischemic stroke, or have the ability to demonstrate where a cerebral hemorrhage has occurred (hemorrhagic stroke).To improve the diagnosis and treatment of blood vessel diseases, such as stroke and aneurysms, we developed fibrinogen aptamer (FA)-functionalized contrast agents, enabling the identification and labelling of blood clots.Fibrin was chosen as the target of interest as it is involved in blood clot formation and is, therefore, a major constituent of aforementioned conditions.Since FA was originally selected to bind fibrinogen, fibrin-binding validation was required.It was hypothesized that FA would retain some binding affinity towards the polymerized form, fibrin, given that most of the structural elements of fibrinogen remain unmodified in the final form.To assess the affinity and selectivity of FA towards nonsolution-based fibrin, FA was tagged with a green emitting fluorophore and fluorescence co-localization was monitored.FA was selective, and binding was immediate upon direct interaction, accumulating to a significant amount within minutes.Solubilized fibrin was also used in a number of binding validation studies, including microscale thermophoresis, isothermal titration calorimetry, and circular dichroism.These techniques were used to calculate the apparent Kd, which was found to be within the acceptable range when compared to the known Kd of FA to fibrinogen.Four different FA-targeted contrast materials were produced, including gadolinium conjugates (Gd(III)-DOTA/NOTA-FA) for MRI, iodinated-FA and FA-functionalized gold nanoparticles (FA-AuNPs) for CT, and FA-functionalized gold-coated iron-oxide

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.003

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.015
GPT teacher head0.248
Teacher spread0.233 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

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Citations0
Published2020
Admission routes1
Has abstractyes

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